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Intensification of paraffin wax separation from oilstocks by static crystallization

机译:静态结晶强化从油料中分离石蜡

摘要

The possibility of paraffin wax separation from the high-boiling slack wax by static crystallization has been studied. Gas chromatographic analysis of individual hydrocarbon composition of the high boiling slack wax and its structural-group compos ition by the method of IR Fourier spectroscopy has been determined, experiments on the de-oiling on installation that simulates the operation of industrial crystallizers has been done. It is established that the de-oiling process of the high-boiling slack wax by static crystallization is obtained tightened in time and economically impractical. It has been proposed to introduce the paraffin oil from low-boiling slack wax as a diluent for the high boiling slack. Physical and chemical analysis of individual raw material components and their mixtures has been determined, the process of de-oiling by static crystallization has been done. The introduction of the paraffin oil from low-boiling slack wax into the high-boiling slack wax reduces the time and the temperature of partial melting phase of static crystallization without worsening the quality of the melt. As a result, the static crystallization goes faster and different technological costs are reduced.
机译:研究了通过静态结晶将石蜡从高沸点松散蜡中分离出来的可能性。通过红外傅里叶光谱法对高沸点松散石蜡的单个烃成分及其结构基组成进行了气相色谱分析,并进行了模拟工业结晶器运行的装置除油实验。已经确定的是,在时间上加紧了在静态上结晶的高沸点松散蜡的除油过程,这在经济上是不切实际的。已经提出从低沸点松散蜡中引入石蜡油作为高沸点松散的稀释剂。确定了各个原料成分及其混合物的物理和化学分析,并完成了通过静态结晶进行除油的过程。从低沸点松散蜡中引入石蜡油到高沸点松散蜡中可减少静态结晶的部分熔融阶段的时间和温度,而不会降低熔体质量。结果,静态结晶进行得更快并且减少了不同的技术成本。

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