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On the microstructure and mechanical property of as-extruded Mg-Gd-Y-Zn alloy with Sr addition

机译:添加Sr的挤压Mg-Gd-Y-Zn合金的显微组织和力学性能

摘要

In this study, microstructure evolutions of Mg-6Gd-3Y-0.1Zn-xSr (x=0, 0.2, 0.6) alloys (named as sample 0Sr, 0.2Sr, 0.6Sr) during heat-treatment and extrusion were investigated. As-cast sample 0Sr contains typical long period stacking ordered (LPSO) phases and MgRE. With Sr addition, amounts of LPSO phases decrease and are gradually replaced by the MgSr phases. After homogenization and annealing treatment, profuse strip LPSO phases readily precipitate in grain interiors of sample 0Sr, while only MgSr and MgRE phases are detected in samples 0.2Sr and 0.6Sr. It suggests that the Sr addition would inhibit LPSO phases. After extrusion, the bimodal grain structures, the bulk and strip LPSO phases are detected in sample 0Sr, which can contribute to providing strengthening and extra strain hardening. In as-extruded sample 0.2Sr, finer recrystallized grain size, bulk MgSr and LPSO phases (micron-scale) and MgRE phase (nano-scale) are found due to the pre-annealing treatment. However, lower amounts of both nano-sized and macro-sized LPSO phases lead to the low ultimate strength (300 MPa). In sample 0.6Sr, the strip LPSO phases are readily formed even though the length and total amounts of LPSO phases decrease. More bulk MgSr phases and LPSO phases are also precipitated, which lead to the more superior yield and ultimate strengths of 0.6Sr sample under higher temperature, as compared with the 0Sr sample.
机译:在这项研究中,研究了Mg-6Gd-3Y-0.1Zn-xSr(x = 0,0.2,0.6)合金(称为样品0Sr,0.2Sr,0.6Sr)在热处理和挤压过程中的组织演变。铸态样本0Sr包含典型的长期堆叠有序(LPSO)相和MgRE。通过添加Sr,LPSO相的数量会减少,并逐渐被MgSr相取代。经过均质化和退火处理后,大量的带状LPSO相易于在样品0Sr的晶粒内部沉淀,而在样品0.2Sr和0.6Sr中仅检测到MgSr和MgRE相。这表明添加Sr会抑制LPSO相。挤出后,在样品0Sr中检测到双峰晶粒结构,块状和条状LPSO相,这可有助于提供强化和额外的应变硬化。在挤压样品0.2Sr中,由于进行了预退火处理,发现了更细的重结晶晶粒尺寸,块状MgSr和LPSO相(微米级)和MgRE相(纳米级)。但是,纳米级和大型LPSO相的含量都较低,导致最终强度低(300 MPa)。在样品0.6Sr中,即使LPSO相的长度和总量减少,也容易形成条状LPSO相。与0Sr样品相比,还会析出更多的块状MgSr相和LPSO相,这导致0.6Sr样品在较高温度下具有更高的屈服强度和极限强度。

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