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Measurement of Curvature Distributions in SiO_2-GaAs Substrate by X-ray Double-Crystal Method

机译:用X射线双晶体法测量SiO_2-GaAs衬底中的曲率分布。

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摘要

A new measurement method for curvature distribution of warped SiO_2-GaAs substrate using differential diffraction angles with respect to a standard rocking curve for flat substrate is presented. These rocking curves are measured by x-ray double crystal method for each reflection from the points which are selected at regular intervals on the specimen by moving the slit placed in front of the specimen. The measurement method is applied at room temperature to three cases of SiO_2-GaAs substrate whose SiO_2 film has been deposited uniformly by CVD at 350℃. These three cases are: i) SiO_2 film deposited on the whole substrate, ii) SiO_2 film partially removed, iii) SiO_2 film completely removed. The results of measurements reveal the following facts. SiO_2-GaAs substrate is warped uniformly independent of the distribution of the lattice defects in the substrate due to the difference of thermal expansion coefficient between SiO_2 film and GaAs crystal. Namely the SiO_2 film on the GaAs crystal is in a state of compression. There is an appreciable difference of the curvature between those for SiO_2 film deposited area and SiO_2 film removed area.
机译:提出了一种相对于平板基板的标准摇摆曲线,利用微分衍射角对翘曲的SiO_2-GaAs基板曲率分布进行测量的新方法。这些摇摆曲线是通过x射线双晶法测量的,通过移动位于样品前面的缝隙,以固定间隔在样品上选择的点对每次反射进行测量。该测量方法在室温下对三种情况下的SiO_2-GaAs衬底进行了测量,这些衬底的SiO_2膜已通过CVD在350℃下均匀沉积。这三种情况是:i)沉积在整个基板上的SiO_2膜,ii)部分除去的SiO_2膜,iii)完全除去的SiO_2膜。测量结果表明以下事实。由于SiO_2膜和GaAs晶体之间的热膨胀系数不同,SiO_2-GaAs衬底均匀地翘曲,而与衬底中晶格缺陷的分布无关。即,GaAs晶体上的SiO 2膜处于压缩状态。 SiO_2膜沉积区域和SiO_2膜去除区域的曲率之间存在明显的曲率差异。

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