Microstructure and mechanical properties of Al2O3/Er3Al5O12 eutectic rods grown by the laser-heated floating zone method

摘要

Eutectic rods of Al2O3-Er3Al5O12 were grown by directional solidification using the laser-heated floating zone method at rates in the range 25-1500mm/h. Their microstructure and mechanical properties (hardness, toughness and strength) were investigated as a function of the growth rate. A homogeneous and interpenetrated microstructure was found in most cases, and interphase spacing decreased with growth rate following the Hunt-Jackson law. Hardness increased slightly as the interphase spacing decreased while toughness was low and independent of the microstructure. The rods presented very high bending strength as a result of the homogeneous microstructure, and their strength increased rapidly as the interphase spacing decreased, reaching a maximum of 2.7GPa for the rods grown at 750mm/h. The bending strength remained constant up to 1300K and decreased above this temperature. The relationship between the microstructure and the mechanical properties was established from the analysis of the microstructure and of the fracture mechanisms. © 2010 Elsevier Ltd.