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Development of pressurized extraction processes for oil recovery from wild almond (Amygdalus scoparia)

机译:开发用于野生杏仁(Amygdalus scoparia)采油的加压萃取工艺

摘要

Wild almond Amygdalus scoparia is a very fruitful tree that is spread over an extensive region of Iran. Considering its high quality oil, the development of clean extraction processes based on the use of compressed fluids is encouraged. In this study, the main factors involved in supercritical fluid extraction (SFE) and pressurized liquid extraction (PLE) of wild almond have been optimized by using two different experimental designs and considering the oil extraction yield as a response variable; effects of time, temperature, pressure, and use of co-solvents were studied for SFE while effects of time, temperature and type of solvent were evaluated for PLE. Results showed that the maximum oil yield using supercritical carbon dioxide was 42 %, obtained under the following conditions: extraction temperature, 40 °C; extraction pressure, 40 MPa; and 10 % ethanol as co-solvent. The optimum extraction yield for PLE was 55 %, which was achieved using ethanol as solvent at 150 °C for 20 min. Lipidomic analysis revealed that the amount of oleic acid in the oil extracted by SFE was higher than those obtained by using other classical procedures. In addition, triacylglycerols constituted more than 98 % of the extracted oils.
机译:野杏仁扁桃(Amygdalus scoparia)是一棵硕果累累的树,遍布伊朗大片地区。考虑到其高质量的油,鼓励基于压缩流体的使用开发清洁的提取工艺。在这项研究中,通过使用两种不同的实验设计并将油的提取产率作为响应变量,对涉及野生杏仁的超临界流体萃取(SFE)和加压液体萃取(PLE)的主要因素进行了优化。研究了时间,温度,压力和助溶剂的使用对SFE的影响,同时评估了时间,温度和溶剂类型对PLE的影响。结果表明,在以下条件下获得的超临界二氧化碳最大产油量为42%:萃取温度40℃;萃取温度40℃。抽气压力40 MPa;和10%的乙醇作为助溶剂。 PLE的最佳提取率为55%,这是在150°C下使用乙醇作为溶剂20分钟实现的。脂质组学分析表明,通过SFE萃取的油中的油酸含量高于使用其他经典方法获得的油酸含量。此外,三酰基甘油占提取油的98%以上。

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