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Liquid-liquid dispersion: effects of dispersed phase viscosity on mean drop size and distribution in stirred vessel

机译:液液分散:分散相粘度对搅拌容器中平均液滴尺寸和分布的影响

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摘要

Drop size distributions in liquid-liquid dispersion are essential in industrial processes as it involve mass and heat transfer between the phases. An experimental investigation was conducted to study liquid-liquid dispersion in stirred vessel. The objective of this experiment is to study the effects of dispersed phase viscosity (moderate to high) on the mean drop size, d32 and drop size distributions at different impeller speed. Different grades of silicone oils were used to create oil in water dispersions with surfactant stabilization and by using Rushton turbine as impeller. Laser diffraction technique (Malvern Mastersizer 2000) was used to measure the mean drop size and distributions. Results showed that mean drop size, d32 are affected by dispersed phase viscosity especially at high dispersed phase viscosity. At low viscosity, higher uniformity of drop sizes was produced as higher drop size distribution curve was obtained and the curve shifted to the left of the graph when theudimpeller speed was increased. Higher viscosity exhibit larger change in d32 as the impeller speed increase (92.76%) compared to low viscosity (44.03%) which is caused by different breakage mechanism.
机译:液-液分散体中的液滴尺寸分布在工业过程中至关重要,因为它涉及相之间的质量和热传递。进行实验研究以研究搅拌容器中的液-液分散。该实验的目的是研究分散相粘度(中到高)对不同叶轮速度下平均液滴尺寸,d32和液滴尺寸分布的影响。使用不同等级的硅油,通过使用Rushton涡轮机作为叶轮,可在具有表面活性剂稳定性的水分散液中形成油。激光衍射技术(Malvern Mastersizer 2000)用于测量平均液滴尺寸和分布。结果表明,平均液滴尺寸d32受分散相粘度的影响,特别是在高分散相粘度下。在低粘度下,由于获得了更高的液滴尺寸分布曲线,因此产生了更高的液滴尺寸均匀性,并且当提高 udimpeller速度时,曲线向图的左侧移动。与较高的粘度相比,随着叶轮转速的提高(92.76%),d32的变化更大,而低粘度(44.03%)则是由不同的断裂机理引起的。

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