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Antibacterial performance of Ag Nanoparticles and AgGO nanocomposites prepared via rapid microwave-assisted synthesis method

机译:快速微波辅助合成法制备的Ag纳米颗粒和AgGO纳米复合材料的抗菌性能

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摘要

Silver nanoparticles and silver-graphene oxide nanocomposites were fabricated using a rapid and green microwave irradiation synthesis method. Silver nanoparticles with narrow size distribution were formed under microwave irradiation for both samples. The silver nanoparticles were distributed randomly on the surface of graphene oxide. The Fourier transform infrared and thermogravimetry analysis results showed that the graphene oxide for the AgNP-graphene oxide (AgGO) sample was partially reduced during the in situ synthesis of silver nanoparticles. Both silver nanoparticles and AgGO nanocomposites exhibited stronger antibacterial properties against Gram-negative bacteria (Salmonella typhi and Escherichia coli) than against Gram-positive bacteria (Staphyloccocus aureus and Staphyloccocus epidermidis). The AgGO nanocomposites consisting of approximately 40 wt. silver can achieve antibacterial performance comparable to that of neat silver nanoparticles.
机译:使用快速和绿色微波辐射合成方法制备了银纳米颗粒和氧化银石墨烯纳米复合材料。在两个样品的微波辐射下均形成了具有窄尺寸分布的银纳米颗粒。银纳米颗粒随机分布在氧化石墨烯的表面。傅里叶变换红外和热重分析结果表明,在银纳米粒子的原位合成过程中,用于AgNP-氧化石墨烯(AgGO)样品的氧化石墨烯被部分还原。银纳米颗粒和AgGO纳米复合材料对革兰氏阴性菌(鼠伤寒沙门氏菌和大肠杆菌)的抗菌性能均比革兰氏阳性菌(金黄色葡萄球菌和表皮葡萄球菌)强。 AgGO纳米复合材料约占40 wt。银可以达到与纯银纳米颗粒相当的抗菌性能。

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