首页> 外文OA文献 >Biosynthesis and characterization of gold and silver nanoparticles by pink guava (psidium guajava) waste extract / Norashikin Ahmad Zamanhuri, Mohamed Syazwan Osman and Rasyidah Alrozi
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Biosynthesis and characterization of gold and silver nanoparticles by pink guava (psidium guajava) waste extract / Norashikin Ahmad Zamanhuri, Mohamed Syazwan Osman and Rasyidah Alrozi

机译:粉红番石榴(psidium guajava)废物提取物/ Norashikin Ahmad Zamanhuri,Mohamed Syazwan Osman和Rasyidah Alrozi的生物合成和金和银纳米颗粒的表征

摘要

There is an increasing commercial demand for nanoparticles due to their wide applicability in various areas such as electronics, catalysis, chemistry, energy and medicine. Metallic nanoparticles are traditionally synthesized by wet chemical techniques, where the chemicals used are quite often toxic and give impact to the human health and environment. Metal nanostructures have unusual physicochemical properties and biological activities compared to their bulk parent materials. In this study, silver and gold nanoparticles (AgNPs and AuNPs) were synthesized from aqueous silver nitrate and auric acid solution respectively, through a simple and eco-friendly route using pink guava waste extract (PGWE) as reductant and stabilizer. The resulting silver and gold nanoparticles were characterized by using Ultraviolet-visible (UV-vis) spectroscopy, Fourier transform infrared (FTIR) spectroscopy and transmission electron microscopy (TEM). AgNPs and AuNPs vary in size according to different amount of PGWE and silver nitrate and auric acid concentration used for the synthesis. Formation of AgNPs and AuNPs was confirmed by the color changed and by surface Plasmon spectra by using Uv-Vis spectrometer as well as absorbance peaks lie between 400 to 500 nm. The silver and gold nanoparticles obtained using this source have particles size in the range of 0- 50 nm. It was found that the increase in silver nitrate and uric acid concentration leads to the increasing size of AgNPs and AuNPs produced.
机译:由于纳米粒子在电子,催化,化学,能源和医学等各个领域的广泛应用,因此对纳米粒子的商业需求不断增长。金属纳米颗粒传统上是通过湿化学技术合成的,其中所使用的化学物质通常有毒,会对人体健康和环境产生影响。与它们的整体母体材料相比,金属纳米结构具有不同寻常的理化性质和生物活性。在这项研究中,使用粉红色番石榴废液提取物(PGWE)作为还原剂和稳定剂,通过简单且生态友好的途径,分别从硝酸银水溶液和金酸溶液中合成了银和金纳米粒子(AgNPs和AuNPs)。所得的银和金纳米粒子通过使用紫外可见(UV-vis)光谱,傅立叶变换红外(FTIR)光谱和透射电子显微镜(TEM)进行表征。 AgNPs和AuNPs的大小会根据用于合成的PGWE和硝酸银的量以及金酸的浓度而变化。通过使用Uv-Vis光谱仪的颜色变化和表面等离激元光谱以及吸收峰在400至500 nm之间,可以确认AgNP和AuNP的形成。使用该来源获得的银和金纳米颗粒的粒度在0-50nm范围内。发现硝酸银和尿酸浓度的增加导致产生的AgNP和AuNP的尺寸增加。

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