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Determination of solidus and liquidus temperatures for S34MnV steel grade by thermal analysis and calculations

机译:通过热分析和计算确定S34MnV钢等级的固相线和液相线温度

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摘要

The paper is devoted to the comparison of the results in the frame of solidus and liquidus temperatures obtained bythermo analytical methods with the generally used empirically based formulas and thermo dynamical Computhermsoftware. The series of thermal analysis measurements of high temperature phase transformations of real steelgrade (S34MnV) under conditions of two analytical devices (Netzsch STA 449 F3 Jupiter; Setaram Multi High TemperatureCalorimeter (MHTC)) were carried out. Two thermo analytical methods were used (DSC and Direct ThermalAnalysis). The different weight of samples was used (2,6 g; 23 g). The liquidus and solidus temperatures for close toequilibrium conditions during heating (DSC: 1 °C/min; 2 °C/min) and during cooling (Direct Thermal Analysis: 1 °C/min) were determined and compared. Then, the discussion on the different values obtained by experiments andempirically based calculation is realised.
机译:本文致力于将通过热分析方法获得的固相线和液相线温度与常用的基于经验的公式和热力学的Computherm软件进行比较。在两个分析设备(Netzsch STA 449 F3 Jupiter; Setaram多高温量热仪(MHTC))的条件下,进行了一系列实际钢级(S34MnV)高温相变的热分析测量。使用了两种热分析方法(DSC和直接热分析)。使用了不同重量的样品(2.6克; 23克)。确定并比较了加热(DSC:1°C / min; 2°C / min)和冷却(直接热分析:1°C / min)附近接近平衡条件的液相线和固相线温度。然后,讨论了通过实验和基于经验的计算获得的不同值。

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