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Characterization of Hot Deformation Behavior and Dislocation Structure Evolution of an Advanced Nickel-Based Superalloy

机译:先进镍基超合金的热变形行为和位错结构演化的表征

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摘要

The hot deformation behavior of an advanced nickel-based Haynes282 superalloy was systematically investigated employing isothermal compression tests in the sub-solvus and super-solvus temperature with various strain rates. The influence of deformation temperature and strain rate on the microstructure was studied by transmission electron microscope. The results reveal that the interaction between work hardening and dynamic softening did not reach equilibrium under lower deformation temperature and higher strain rate. The active energy of alloy is around 537.12 kJ/mol and its hot deformation constitutive relationship equation was expressed. According to the processing map and microstructure observations, two unsafe flow instability domains should be avoided. The optimum hot processing condition for homogeneous and fine dynamic recrystallization grains are obtained. TEM micrograph observations indicated that deformation temperature and strain rate affected recrystallization by affecting the evolution of dislocation substructures within the alloy. The nucleation and growth of DRX grains can be promoted by the relatively high deformation temperature and low strain rate. The main mechanism of dynamic recrystallization nucleation preferred to discontinuous dynamic recrystallization and the typical feature of discontinuous dynamic recrystallization showed grain boundary migration nucleation. The findings improve the understanding of hot deformation behavior and dislocation substructures evolution of the superalloy, which benefits the accurate control of microstructures of nickel-based superalloys, and tailors the properties of final components used in the land-based gas turbine.
机译:通过各种应变速率系统地研究了先进镍基Haynes282高温合金的热变形行为在亚溶剂和超级溶剂温度下采用等温压缩试验。通过透射电子显微镜研究了变形温度和应变率对微观结构的影响。结果表明,工作硬化和动态软化之间的相互作用在较低变形温度和较高的应变率下没有达到平衡。合金的活性能量约为537.12kJ / mol,并且其热变形本构关系方程被表达。根据处理地图和微观结构观察,应避免两个不安全的不稳定域。获得了均匀和细致的重结晶晶粒的最佳热处理条件。 TEM显微照片观察表明,通过影响合金内的位错子结构的演变,变形温度和应变率受重结晶。 DRX晶粒的成核和生长可以通过相对较高的变形温度和低应变速率促进。动态重结晶成核的主要机理优于不连续的动态再结晶和不连续动态再结晶的典型特征显示晶界迁移成核。该研究结果提高了高温合金的热变形行为和脱位子结构演化的理解,这有利于镍基超合金的微观结构的精确控制,并裁定在陆基燃气轮机中使用的最终部件的性能。

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