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Preparation of biodiesel from waste cooking oil and refines bleached deodorized oil using single step batch transesterification process with the aid of KOH as the catalyst

机译:从废食用油中制备生物柴油,并在KOH的辅助下,通过单步间歇酯交换工艺精制漂白的脱臭油。

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摘要

Biodiesel is a cleaner burning diesel replacement fuel processed from natural, renewable derived from biological sources such as waste cooking oil and refined bleached deodorized palm oil. The type of process that needs to be done to produce biodiesel is called transesterification. The transesterification of waste cooking oil and refined bleached deodorized palm oil with short-chain alcohols, in the presence of base-catalyst potassium hydroxide (KOH) and methanol as solvent, by means of single step batch transesterification process in order to obtain biodiesel fuel was studied. The reaction has been done in water bath. The process variables that been investigated are catalyst concentration and reaction time. The variables that are fixed throughout the whole experiment were molar ratio of methanol to raw oil with 6: 1, reaction temperature at 40oC and mixing degree of mechanical stirrer at 1300 rpm. This paper also studied the combustion characteristic which is the carbon monoxide emission between WCO and RBD to be compared with conventional diesel, and determined the optimal transesterification reaction conditions that produce the maximum methyl ester content or purity and biodiesel yield. The best result for highest yield and highest purity is at 60 minutes reaction time and using 1.5% catalyst concentration.
机译:生物柴油是一种清洁燃烧的柴油替代燃料,它是用生物废料和精制漂白脱臭棕榈油等生物资源衍生的天然可再生资源加工而成的。生产生物柴油所需完成的过程类型称为酯交换反应。在碱催化剂氢氧化钾(KOH)和甲醇为溶剂的情况下,通过一步分批酯交换工艺将废食用油和精制漂白脱臭棕榈油与短链醇进行酯交换反应,从而获得生物柴油燃料。研究。反应已在水浴中完成。研究的过程变量是催化剂浓度和反应时间。在整个实验中固定的变量是甲醇与原料油的摩尔比为6:1,反应温度为40oC,机械搅拌器的混合度为1300 rpm。本文还研究了燃烧特性,即WCO和RBD之间的一氧化碳排放量,以与常规柴油进行比较,并确定了产生最大甲酯含量或纯度和生物柴油收率的最佳酯交换反应条件。最高收率和最高纯度的最佳结果是在60分钟的反应时间下,使用1.5%的催化剂浓度。

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    Mahfuzah Mansor;

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  • 年度 2009
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