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Evaluation on the Effects of Wax Inhibitor and Optimization of Operating Parameters For Wax Deposition in Malaysian Crude Oil

机译:马来西亚原油蜡抑制剂的效果评价和蜡沉积工艺参数的优化

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摘要

The complex phenomenon of wax deposition subject to thermal gradient in crude oil is one of the biggest challenges in petroleum industry. In this comparative study, two inhibitors which were poly(ethylene-co-vinyl acetate) (EVA) and xylene were investigated in terms of rate of wax deposition in Malaysian crude oil using one-factor-at-a-time (OFAT) approach and cold finger methods. Stirring rate and cold finger temperature were optimized using response surface methodology (RSM) after being investigated using OFAT. It can be concluded that EVA had higher capability of reducing wax in two different conditions where the minimum point of wax reduction was found at 400 rpm with 63.5% paraffin inhibition efficiency (PIE) and 10°C with 64.7% of PIE. The amount of waxes collected for each parameter were 0.35 and 0.49 g, respectively. To minimize the wax deposit amount, RSM approach was applied using rotatable central composite design (CCD). The result shows that the amount of wax deposit decreased significantly with the increase of temperature and the stirring rate which were set at 400 rpm and 19°C, rescpectively. The amount of wax deposit was successfully reduced to the minimum value of 0.0095 g after the optimization.
机译:原油中受热梯度影响的蜡沉积复杂现象是石油工业面临的最大挑战之一。在这项比较研究中,使用一次一因素分析(OFAT)的方法研究了两种抑制剂,即聚(乙烯-乙酸乙烯酯共聚物)(EVA)和二甲苯,对马来西亚原油中蜡沉积速率的影响和冷手指方法。使用OFAT研究后,使用响应表面方法(RSM)优化搅拌速度和手指冷感。可以得出结论,在两种不同的条件下,EVA都有较高的蜡还原能力,在400 rpm时,蜡的最小还原点为63.5%的石蜡抑制效率(PIE),在10°C时为64.7%的PIE。每个参数收集的蜡量分别为0.35和0.49 g。为了最大程度地减少蜡沉积量,使用可旋转中央复合设计(CCD)来应用RSM方法。结果表明,蜡的沉积量随温度和搅拌速率的增加而显着减少,温度和搅拌速率分别设定为400 rpm和19°C。优化后,蜡沉积量成功减少到最小值0.0095 g。

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