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Extraction and characterization of essential oil from ginger (Zingiber Officinale Roscoe) and lemongrass (Cymbopogon Citratus) by microwave-assisted hydrodistillation (MAHD)

机译:微波辅助加氢蒸馏(MAHD)从姜(Zingiber Officinale Roscoe)和柠檬草(Cymbopogon Citratus)中提取和表征精油

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摘要

Microwave-assisted hydrodistillation (MAHD),an advanced distillation method that take advantage of microwave heating with the conventional hydrodistillation,recently been widely attended for the extraction of essential oil from medicinal plants and herbs due to its economic and green technology. One way in maximizing the efficiency of a method is optimizing its parameter condition to obtain maximum yield. In that case,this study was carried out to investigate the performance of MAHD in the extraction of essential oil from Ginger (Zingiber Officinale Roscoe) and Lemongrass (Cymbopogon citratus).The effect of three main factors which were microwave power,extraction time and water to raw material ratio were investigated to optimize the extraction operating conditions for obtaining maximum oil yield.As a result the best condition that has been determined for maximum essential oil production were under 250 W microwave power for 90 minutes at water to raw material ratio of 8:1. This optimum condition was finalized based on its maximum yield from Ginger (Zingiber Officinale Roscoe) and Lemongrass (Cymbopogon citratus) which were 0.85% (w/w) and 1.37%(w/w),respectively.Then,the oil samples at different extraction time were analyzed to evaluate its quality by determined its chemical constituent through GC-MS.The main components detected in the essential oil of Ginger (Zingiber Officinale Roscoe) were Borneol,β-Bisabolene,Cineole,α-Cedrene,α-Curcumene,β-Farnesene(E),β-Sesquihelladiene,β-Thujene and Zingiberene. Wherelse, the main components in the essential oil of Lemongrass (Cymbopogon citratus) were Citral,Geranic Acid,Geranyl Acetate,Linalool, Neric acid, (Z) Citral,β-mycrene and β-Thujene.The dominant component in the essential oil of Ginger (Zingiber Officinale Roscoe) and Lemongrass (Cymbopogon citratus) were Zingiberene and Citral, respectively.The maximum oil yield from Ginger (Zingiber Officinale Roscoe)and Lemongrass (Cymbopogon citratus) were obtained at shorter extraction period without significant affect on their chemical constituents.This may prove MAHD as a cost effective method and also expected would bring volume of worth in the essential oil production industry.
机译:微波辅助加氢蒸馏(MAHD)是一种利用传统加氢蒸馏技术利用微波加热的先进蒸馏方法,由于其经济和绿色技术,最近被广泛用于从药用植物和草药中提取精油。最大化方法效率的一种方法是优化其参数条件以获得最大产量。在这种情况下,本研究旨在研究MAHD在从生姜(Zingiber Officinale Roscoe)和柠檬草(Cymbopogon citratus)提取精油中的性能。微波功率,提取时间和水三个主要因素的影响对原料比进行了研究,以优化提取操作条件以获得最大的油收率。因此,确定最大香精油产量的最佳条件是在水功率为8的250 W微波功率下90分钟:1。根据姜(Zingiber Officinale Roscoe)和柠檬草(Cymbopogon citratus)的最高产量分别确定最佳条件,分别为0.85%(w / w)和1.37%(w / w)。通过气相色谱-质谱法(GC-MS)确定其化学成分,分析了提取时间,以评价其质量。生姜中的主要成分为冰片中的冰片,冰片中的β-异丁香烯,肉桂脂,α-雪松烯,α-姜黄素, β-法呢烯(E),β-倍半萜二烯,β-丁二烯和姜黄烯。其中,柠檬草(Cymbopogon citratus)香精油的主要成分为柠檬醛,香叶酸,香叶酸乙酸酯,利那洛尔,神经酸,(Z)柠檬醛,β-丁烯和β-丁二烯。姜(Zingiber Officinale Roscoe)和柠檬香茅(Cymbopogon citratus)分别为姜黄素和柠檬醛,而姜(Zingiber Officinale Roscoe)和柠檬香茅(Cymbopogon citratus)的最大产油量在较短的提取时间内获得,而对其化学成分没有明显影响。这可能证明MAHD是一种经济有效的方法,并且还有望在香精油生产行业中带来巨大的价值。

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    Ranitha Mathialagan;

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  • 年度 2012
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