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Device and method of optically orienting biaxial crystals for sample preparation

机译:使样品制备中的双轴晶体光学取向的装置和方法

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摘要

An optical instrument we refer to as the “biaxial orientation device” has been developed for finding the optical plane, acute bisectrix, and obtuse bisectrix in biaxial crystals by means of optically aligning conoscopically formed melatopes and measuring the angular coordinates of the melatopes, where the angular values allow for determination of the optical plane containing the optical axes using a vector algebra approach. After determination of the optical plane, the instrument allows for the sample to be aligned in the acute bisectrix or obtuse bisectrix orientations and to be transferred to a simple mechanical component for subsequent grinding and polishing, while preserving the orientation of the polished faces relative to the optical plane, acute bisectrix, and obtuse bisectrix during the grinding and polishing process. Biaxial crystalline material samples prepared in the manner are suitable for accurate spectroscopic absorption measurements in the acute bisectrix and obtuse bisectrix directions as well as perpendicular to the optical plane.
机译:已经开发出一种我们称为“双轴定向设备”的光学仪器,用于通过光学排列圆锥形形成的黑斑表面并测量黑斑表面的角坐标来发现双轴晶体中的光学平面,锐角双眼形和钝双眼形。角度值允许使用矢量代数方法确定包含光轴的光学平面。在确定了光学平面之后,该仪器允许将样品以锐二等分或钝二等分的方向对齐,并转移到简单的机械组件中进行后续的研磨和抛光,同时保留抛光面相对于抛光面的方向。在研磨和抛光过程中,光学平面,急性双裂和钝双裂。以这种方式制备的双轴晶体材料样品适合于在急性双裂和钝双裂方向以及垂直于光学平面的精确光谱吸收测量。

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