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Portable Gas Analyzer Based on Fourier Transform Infrared Spectrometer for Patrolling and Examining Gas Exhaust

机译:基于傅里叶变换红外光谱仪的便携式气体分析仪进行巡逻和检查气体排气

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摘要

Aimed at monitoring emission of organic gases such as CH4, C2H6, C3H8, iso-C4H10, n-C4H10, C2H4, C3H6, C2H2, CO, and CO2, from coal mines, petroleum refineries, and other plants, a Fourier Transform Infrared (FT-IR) spectrometer was used to develop a portable gas analyzer for patrolling and examining gas exhaust. Firstly, structure of the instrument was introduced. Then, a spectral analysis approach was presented. Finally, instrument was tested with standard gases and with actual gases emitted from a petroleum refinery. For the latter test, a gas chromatograph (GC) was used as a reference instrument. The test results showed that the detection limit of every component of analyte was less than 10 × 10−6. The maximum test error of every analyte was less than 15 × 10−6 when its practical concentration was no more than 500 × 10−6. A final comparison showed that the result curves of analytes obtained with FT-IR spectrometer almost overlapped with those obtained with GC, and their resulting noise was less than 6.4% when the practical gas concentration was above 100 × 10−6. As a result, our instrument was suitable to be used as a portable instrument for monitoring exhaust gases.
机译:在监测有机气体如CH 4,C 2 H 6,C 3 H 8,异C4H10,正C4H10,C2H4,C3H6,C2H2,CO,和CO 2的排放量的目的,从煤矿,石油精炼厂,和其他植物中,傅立叶变换红外( FT-IR)光谱仪用于开发便携式气体分析仪,用于巡逻和检查气排气排气。首先,介绍了仪器的结构。然后,提出了一种光谱分析方法。最后,用标准气体测试仪器,并从石油炼油厂发出的实际气体。对于后一试,将气相色谱仪(GC)用作参考仪器。测试结果表明,分析物的每个组分的检测限小于10×10-6。当其实际浓度不超过500×10-6时,每个分析物的最大测试误差小于15×10-6。最后的比较表明,用FT-IR光谱仪获得的分析物的结果曲线几乎与GC获得的那些,当实际气体浓度高于100×10-6时,它们的所得噪声小于6.4%。结果,我们的仪器适合用作用于监测废气的便携式仪器。

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