Die Struktur von DL-μ-hydroxo-di-μ-nitro-bis(triamminkobalt)(3+)-trichlorid-hydrat

摘要

DL-μ-Hydroxo-di-μ-nitro-bis(triamminecobalt)(3 + )-trichloride hydrate, [(NH_3)_3Co(OH)(N0_2hCo(NH_3)_3]Cl_3. H_20, crystallizes in the monoclinic space group P2_1/c with ɑ = 9·70, b = 6-73, c = 24·57 Å and β = 104·3°; there are four formula units in the cell. The structure was determined by the heavy-atom method and refined by three-dimensional least-squares calculations. Theudfinal R index for 1397 observed reflections of non-zero weight is 0·067.