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Fabrication of flourine doped tin oxide with different volume of solvents on FTO seed layer by hydrothermal method

机译:水热法在FTO种子层上制备不同溶剂量的掺氟氧化锡

摘要

Flourine doped tin oxide films were synthesized by using hydrothermal method with different volume of solvents. The thin film growth was carried out by fixing the concentration of tin and fluorine element precursors by only varying their solvents which were 2-propanol and DI water. The fabrication of FTO thin film by using mineral salt group as tin precursor with hydrothermal method on soda lime glass showed that the nanostructured growth did not distribute largely and took longer time. The seed layer of FTO has been used to overcome these problems thus the thin film growth distributed largely in short time. These experiments were conducted at a constant of hydrothermal temperature and reaction time which were 150°C and 5 h respectively. The result showed that, there was a change on the surface morphology in the formation of FTO films. The minimum value of sheet resistance was 0.1475 Ω/sq which was obtained using 65 mL of 2-propanol and 20 mL of DI water was lower than sheet resistance of commercial FTO films of 01693 Ω/sq. This fabricated FTO films showed a good transparency with higher of transmittance than 80%. The experimental findings suggested that 65 mL amount of 2-propanol and 20 mL of DI water in precursor solutions could produce the better of FTO performance than commercial FTO.
机译:采用水热法,在不同体积的溶剂中合成了氟掺杂的氧化锡薄膜。通过仅改变它们的溶剂为2-丙醇和去离子水来固定锡和氟元素前体的浓度,从而进行薄膜生长。在钠钙玻璃上水热法以无机盐基团为锡前驱体制备FTO薄膜表明,纳米结构的生长分布不大,耗时较长。 FTO的种子层已经用于克服这些问题,因此薄膜的生长在短时间内大量分布。这些实验是在恒定的水热温度和反应时间(分别为150°C和5 h)下进行的。结果表明,在FTO膜的形成中,表面形态发生了变化。使用65mL的2-丙醇和20mL的DI水获得的薄层电阻的最小值为0.1475Ω/ sq,低于市售FTO膜的01693Ω/ sq的薄层电阻。制成的FTO薄膜显示出良好的透明性,透射率高于80%。实验结果表明,前体溶液中65毫升的2-丙醇和20毫升的去离子水可以产生比商业FTO更好的FTO性能。

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