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Impact of Ion Irradiation upon Structure and Magnetic Properties of NANOPERM-Type Amorphous and Nanocrystalline Alloys

机译:离子照射对纳米膜晶型无定形和纳米晶合金结构和磁性的影响

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摘要

Structural modifications and their impact upon magnetic properties are studied in amorphous and nanocrystalline NANOPERM-type 57Fe75Mo8Cu1B16 alloy. They are introduced by irradiation with 130 keV N+ ions to the total fluencies of up to 2.5 × 1017 ions/cm2 under different cooling conditions. Increased temperature during the irradiation triggers formation of nanocrystallites of bcc-Fe in those subsurface regions that are affected by bombarding ions. No crystallization occurs when good thermal contact between the irradiated sample and a sample holder is assured. Instead, structural rearrangement which favours development of magnetically active regions was determined by the local probe methods of Mössbauer spectrometry. Dipole magnetic interactions dominate in subsurface regions on that side of the ribbons which was exposed to ion irradiation. Nevertheless, structural modifications demonstrate themselves also via macroscopic magnetic parameters such as temperature dependence of magnetization, Curie temperature, and hysteresis loops. Impact of only the temperature itself to the observed effects is assessed by the help of samples that were subjected just to heat treatment, that is, without ion irradiation.
机译:在无定形和纳米晶纳米膜中的57Fe75mO8Cu1b16合金中研究了结构改变及其对磁性的影响。在不同冷却条件下,通过用130keV n +离子的辐射引入,通过130keV n +离子的辐射引入,其总流量高达2.5×1017离子/ cm2。在受轰击离子影响的那些地下区域中,在照射期间的温度增加触发BCC-FE的纳米晶体。当照射样品和样品架之间的良好热接触确保了时,不会发生结晶。相反,通过Mössbauer光谱法的局部探针方法确定了涉及磁活性区域的结构的结构重排。偶极磁性相互作用在接触到离子照射的带子的地下区域上占据主导地位。然而,结构修改还通过宏观磁性参数展示自己,例如磁化,居里温度和滞后环的温度依赖性。仅通过对热处理的样品的帮助来评估仅温度本身对观察到的效果的影响,即没有离子辐射。

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