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Determination of the extraction efficiency of polycyclic aromatic hydrocarbons from airborne particulate matter

机译:从空机颗粒物质中测定多环芳烃的提取效率

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摘要

Polycyclic aromatic hydrocarbons are common environmental pollutants that reach atmosphere in the form of aerosol adsorbed on soot, ash and dust. Having in mind its carcinogenic and mutagenic effects most countries have regulations concerning their estimation in environmental samples. In this work we have investigated extraction efficiency of several polycyclic aromatic hydrocarbons from flying particles collected on glass fibber filters. Efficiency of extraction of different duration in Soxhlet apparatus, ultrasonic bath and boiling toluene under reflux were compared. It has been established that compounds having two or three condensed rings are lost during evaporation of toulene that was used as a solvent. For compounds having five or more condensed rings extraction in ultrasonic bath and boiling toluene using magnetic stirrer and reflux are the most efficient.
机译:多环芳烃是常见的环境污染物,可在吸附在烟灰,灰和粉尘上的气溶胶形式的气氛。考虑到其致癌性和致突变性的效果大多数国家都有关于他们在环境样本中估算的规定。在这项工作中,我们研究了从收集在玻璃纤维过滤器上收集的颗粒的多个多环芳烃的提取效率。索氏素装置中不同持续时间的提取效率,反流下的超声浴和沸腾甲苯。已经确定,在用作溶剂的甘油中蒸发过程中,具有两个或三个稠环的化合物损失。对于使用磁力搅拌器和回流具有超声浴和沸腾甲苯的五个或更多个冷凝环萃取的化合物是最有效的。

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