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Molybdenum oxide nanocolloids prepared by an external field-assisted laser ablation in water

机译:通过外部现场辅助激光烧蚀在水中制备的氧化钼纳米核苷酸

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摘要

he synthesis of extremely stable molybdenum oxide nanocolloids by pulsed laser ablation was studied. This green technique ensures the formation of contaminant-free nanostructures and the absence of by-products. A focused picosecond pulsed laser beam was used to ablate a solid molybdenum target immersed in deionized water. Molybdenum oxide nearly spherical nanoparticles with dimensions within few nanometers (20-100 nm) are synthesized when the ablation processes were carried out, in water, at room temperature and 80°C. The application of an external electric field during the ablation process induces a nanostructures reorganization, as indicated by Scanning-Transmission Electron Microscopy images analysis. The ablation products were also characterized by some spectroscopic techniques: conventional UV-vis optical absorption, atomic absorption, dynamic light scattering, micro-Raman and X-ray photoelectron spectroscopies. Finally, NIH/3T3 mouse fibroblasts were used to evaluate cell viability by the sulforhodamine B assay
机译:研究了通过脉冲激光烧蚀来合成极稳定的氧化钼纳米胶质。这种绿色技术确保了无污染纳米结构的形成和副产物的不存在。聚焦皮秒脉冲激光束用于烧成浸入去离子水中的固体钼靶。当在水中进行烧蚀过程,在室温和80℃下,在氧化氢气,在水中进行时,合成氧化钼几乎是球形纳米颗粒(20-100nm)。如扫描透射电子显微镜图像分析所示,在消融过程中施加外部电场诱导纳米结构重组。消融产品的特征在于一些光谱技术:常规的UV-Vis光学吸收,原子吸收,动态光散射,微拉曼和X射线光电子谱。最后,NIH / 3T3小鼠成纤维细胞用于通过苏尔磺胺胺B测定来评估细胞活力

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