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Effect of Hydrochloric Acid Concentration on Morphology of Polyaniline Nanofibers Synthesized by Rapid Mixing Polymerization

机译:盐酸浓度对快速混合聚合合成的聚苯胺纳米纤维形态的影响

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摘要

Polyaniline (PANI) nanofibers with diameters ranging from 60 nm to 190 nm were successfully synthesized by rapid mixing polymerization method at room temperature. The effects of synthesis conditions such as concentration of hydrochloric acid (HCl), ammonium persulfate (APS), and aniline monomer (Ani) on the morphology of PANI nanofibers were investigated using scanning electron microscopy (SEM). FTIR and UV-Vis analysis were performed to characterize the PANI nanofibers. The effect of polymerization time and electrical properties of PANI nanofibers was also discussed. A rapid mixing polymerization method is found to be advantageous in producing bulk quantities of nanofibers.
机译:通过在室温下快速混合聚合方法成功地合成了直径为60nm至190nm的直径的聚苯胺(PANI)纳米纤维。使用扫描电子显微镜(SEM)研究了合成条件(如盐酸(HCl),过硫酸铵(APS)和苯胺单体(ANI)的浓度浓度的效果,对Pani纳米纤维的形态进行研究。进行FTIR和UV-VIS分析以表征PANI纳米纤维。还讨论了Pani纳米纤维的聚合时间和电性能的影响。发现快速混合聚合方法在生产大量纳米纤维中是有利的。

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