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Preparation and characterization of diamond–silicon carbide–silicon composites by gaseous silicon vacuum infiltration process

机译:气态硅真空渗透法制备金刚石-碳化硅-硅复合材料及其表征

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摘要

Diamond–SiC–Si composites have been prepared using gaseous silicon vacuum infiltration. The evolution of the phases and microstructures of the composites have been analyzed using X-ray diffraction technique and scanning electron microscopy. It has been found that the diamond–SiC–Si composite is composed of β-SiC, diamond, and residual Si. The diamond particles were distributed homogeneously in the dense matrix of the composites. Besides, the effects of particle size and content of diamond on the properties of diamond–SiC–Si composites have been analyzed. The thermal conductivity of the composites increases with particle size and content of diamond. When the particle size and content of diamond are 300 µm and 80 wt %, respectively, the thermal conductivity of the composites approaches the value of 280 W·m⁻¹·K⁻¹.
机译:金刚石-SiC-Si复合材料是利用气态硅真空渗透法制备的。使用X射线衍射技术和扫描电子显微镜分析了复合物的相和微观结构的演变。已经发现,金刚石-SiC-Si复合材料由β-SiC,金刚石和残留的Si组成。金刚石颗粒均匀地分布在复合材料的致密基体中。此外,分析了金刚石的粒度和含量对金刚石-SiC-Si复合材料性能的影响。复合材料的热导率随金刚石的粒径和含量而增加。当金刚石的粒径和含量分别为300μm和80wt%时,复合材料的热导率接近280W·m-1·K-1的值。

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