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Diamond-max ceramics bonding phase composites – phases and microstructure analysis

机译:Diamond-max陶瓷粘结相复合材料–相和微结构分析

摘要

The possibility for improving the thermal stability of polycrystalline materials based on diamond (PCD) is to reduce the content of cobalt. Diamond compacts without cobalt phases with Ti3₃iC₂ і Cr₂AlC prepared using the method of self-propagating high-temperature synthesis (SHS). The resulting compacts with 20 wt. % of the above phases were exposed to high pressure and temperature in order to further consolidate the structure by sintering. Sintering was performed at 8±0.2 GPa and 1950±50 °C. Phase composition and microstructural study of the original compacts and the composites made by X-ray diffraction (XRD) and scanning electron microscopy (SEM).
机译:改善基于金刚石的多晶材料(PCD)的热稳定性的可能性是减少钴的含量。用自蔓延高温合成(SHS)方法制备的Ti3 + iC 2-Cr 2 AlC无钴相的金刚石压块。所得的压坯为20重量%。 %的上述相暴露于高压和高温,以通过烧结进一步巩固结构。在8±0.2GPa和1950±50℃下进行烧结。 X射线衍射(XRD)和扫描电子显微镜(SEM)制备的原始压坯和复合材料的相组成和微观结构研究。

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