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A facile hydrothermal approach for catalytic and optical behavior of tin oxide- graphene (SnO2/G) nanocomposite

机译:氧化锡 - 石墨烯(SNO2 / G)纳米复合材料的催化和光学性能的容易水热方法

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摘要

A cost-effective, facile hydrothermal approach was made for the synthesis of SnO2/graphene (Gr) nano-composites. XRD diffraction spectra clearly confirmed the presence of tetragonal crystal system of SnO2 which was maintaining its structure in both pure and composite materials' matrix. The stretching and bending vibrations of the functional groups were analyzed using FTIR analysis. FESEM images illustrated the surface morphology and the texture of the synthesized sample. HRTEM images confirmed the deposition of SnO2 nanoparticles over the surface of graphene nano-sheets. Raman Spectroscopic analysis was carried out to confirm the in-plane blending of SnO2 and graphene inside the composite matrix. The photocatalytic performance of the synthesized sample under UV irradiation using methylene blue dye was observed. Incorporation of grapheme into the SnO2 sample had increased the photocatalytic activity compared with the pure SnO2 sample. The electrochemical property of the synthesized sample was evaluated.
机译:为合成SnO2 /石墨烯(GR)纳米复合材料制备了成本效益的容易的水热方法。 XRD衍射光谱清楚地证实了SnO2的四方晶体系统的存在,其在纯和复合材料的基质中保持其结构。使用FTIR分析分析官能团的拉伸和弯曲振动。 FeSEM图像说明了合成样品的表面形态和纹理。 HRTEM图像证实了SnO2纳米颗粒在石墨烯纳米片表面上沉积。进行拉曼光谱分析,以确认复合基质内的SnO2和石墨烯的面内混合。观察到使用亚甲基蓝染料在UV照射下合成样品的光催化性能。与纯SnO2样品相比,将图形掺入SnO 2样品中的光催化活性增加。评价合成样品的电化学性质。

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