首页> 外文OA文献 >On the Micromixing Behavior of a Spinning Disk Reactor for Metallic Cu Nanoparticles Production
【2h】

On the Micromixing Behavior of a Spinning Disk Reactor for Metallic Cu Nanoparticles Production

机译:金属Cu纳米粒子生产纺丝磁盘反应器的微混凝行为

代理获取
本网站仅为用户提供外文OA文献查询和代理获取服务,本网站没有原文。下单后我们将采用程序或人工为您竭诚获取高质量的原文,但由于OA文献来源多样且变更频繁,仍可能出现获取不到、文献不完整或与标题不符等情况,如果获取不到我们将提供退款服务。请知悉。

摘要

The interest in producing copper nanoparticles is high, mainly due to their enhanced properties, a wide range of possible and different applications, and the possibility for their use in the framework of catalysis. The purpose of this study is to synthesize copper nanoparticles by chemical reduction of copper sulfate with L-ascorbic acid and sodium borohydride capable to eliminate free radicals providing an antioxidant environment promoting pure copper nuclei formation. The micromixing conditions necessary for the nanoparticles production are provided by a spinning disk reactor (SDR). Relevant operational parameters, such as the disk speed velocity and the position of the reactant injectors, will lead to different product outcomes. The latter was checked by means of a dynamic light scattering instrument (DLS). At the end, depending on the adopted operating conditions, the SDR was able to produce particles between 16 nm and 39 nm, with a particle size distribution (PSD) characterized by a narrow, monomodal plot. In comparison to the smallest particles obtained in a stirred reactor tank, that is, 132 nm, the obtained results appear to be very promising.
机译:生产铜纳米粒子的兴趣高,主要是由于其增强的性质,各种可能和不同的应用,以及它们在催化框架中使用的可能性。本研究的目的是通过用L-抗坏血酸和硼氢化钠的硫酸铜化学减少铜纳米颗粒,能够消除自由基,提供促进纯铜核形成的抗氧化环境。纳米颗粒生产所需的微混凝条件由纺丝盘反应器(SDR)提供。相关的操作参数,例如磁盘速度和反应物喷射器的位置,将导致不同的产品结果。通过动态光散射仪器(DLS)检查后者。最后,根据所采用的操作条件,SDR能够在16nm和39nm之间产生颗粒,其特征在于狭窄的单峰曲线,其特征在于粒径分布(PSD)。与在搅拌反应器罐中获得的最小颗粒相比,即132nm,所得结果似乎非常有前景。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
代理获取

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号