THE DETERMINATION OF STEROID ALCOHOLS WITH ACETIC ANHYDRIDE C14

摘要

The preparation of acetic anhydride-C of two levels of specific activity is described. The preparation of derivatives of alcoholic steroids enabled sub microgram analysis of pure androsterone, dehdroepiandrosterone, cortisone, and cotticosterone. This materially decreases the cost of the analysis. Mixtures of these compounds were acetylated and measured.