Least Squares Refinement of Centrosym-Metric Structures Including Anisotropic Thermal Parameters (1) (AND) a First Refinement of the Structure of Cupric Tropolone (11)

摘要

I, A program designed for the IBM704 computer is described. It carries out least squares refinement of crystal structure parameters, including anisotropic temperature parameters, for Centro symmetric crystals.nII. New measurements of the intensities of the (hkO)nzone of reflections from cupric trampolines have been made. The structure has been refined by the method of least squares, using the program of I, in this zone. The results indicate that in cupric tropolone the ring is irregular and slightly puckered.