Assay of TATB by HPLC, Precision and Accuracy Study

摘要

The precision and accuracy of a HPLC method for the assay of TATB were determined. The average relative standard deviation (RSD) of the method is 0.57%. Only one TATB sample gave an RSD value greater than 1% and that sample was made by an experimental process using nitrobenzene as the amination solvent rather than toluene. The accuracy error of the analysis averaged 0.62%. (ERA citation 04:049088)