A Lattice Parameter Method for Determining the Composition of NH4Cl04/KCl04 Solid Solution

摘要

The lattice parameters of eight samples of NH4ClO4, KClO4, and NH4ClO4/KClO4 solid solutions were determined by photographic powder x-ray diffraction. With the aid of a computer, the parameters were calculated utilizing both least squares analysis and successive approximations techniques. The data indicated that, at the present time, the method could be used for analysis of NH4ClO4/KClO4 solid solutions containing less than 20 mole percent KClO4. (Author)