A high resolution X-ray diffraction study has been performed on a single crystal of USb0.8Te0.2. At room temperature this material has the cubic FCC (NaCl) structure. On cooling through the Neel point of similar to 205 K USb0.8Te0.2 is known to enter a triple-q antiferromagnetic phase. Below T-C similar to 175 K USb0.8Te0.2 is a ferromagnet with net magnetisation along the [111] body diagonal. Four-circle X-ray scattering data from high-symmetry {h0h} and {hhh} reflections are presented as a function of temperature. We confirm that this magnetisation directly leads to a magneto-elastic distortion of the crystal lattice with a rhombohedral extension along the [111] body diagonals. At 130 K, this distortion is found to correspond to a rhombohedral bond angle of alpha = 89.856 degrees +/- 0.004 degrees consistent with previous results. In this single-crystal study we also present evidence for additional associated effects which we attribute to inter-grain stresses and sample mosaic structure.
展开▼
机译:对USb0.8Te0.2单晶进行了高分辨率X射线衍射研究。在室温下,该材料具有立方FCC(NaCl)结构。在冷却通过类似于205 K的Neel点时,已知USb0.8Te0.2进入三重q反铁磁相。在T-C下方类似于175 K USb0.8Te0.2的是一个沿[111]体对角线具有净磁化强度的铁磁体。来自高对称{h0h}和{hhh}反射的四圆X射线散射数据表示为温度的函数。我们确认,这种磁化直接导致沿[111]体对角线具有菱形延伸的晶格的磁弹性变形。在130 K处,发现该变形对应于与以前的结果一致的α= 89.856度+/- 0.004度的菱面体结合角。在这个单晶研究中,我们还提供了其他相关效应的证据,这些效应归因于晶粒间应力和样品镶嵌结构。
展开▼