A facile approach for the synthesis of alpha-halogenated alkylidenediphosphonates by reaction of alkyllithium with chlorophosphate and halogen reagent

Lai CB; Xi CJ; Feng YP

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A facile approach for the synthesis of alpha-halogenated alkylidenediphosphonates by reaction of alkyllithium with chlorophosphate and halogen reagent

机译：一种通过烷基锂与氯磷酸盐和卤素试剂反应合成α-卤代亚烷基二膦酸酯的简便方法

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摘要

Alkyllithium reacts with chlorophosphate to generate the alpha-lithioalkylidenediphosphonate, which further reacts with halogen reagents to afford corresponding alpha-halogenated alkylidenediphosphonates.

机译：烷基锂与氯代磷酸反应生成α-硫代亚烷基二膦酸酯，其进一步与卤素试剂反应，得到相应的α-卤代亚烷基二膦酸酯。

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《Phosphorus, Sulfur, and Silicon and the Related Elements》 |2004年第3期|共7页
作者
Lai CB; Xi CJ; Feng YP;
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正文语种 eng
中图分类非金属元素及其化合物;
关键词
alpha-lithio-alkylidenediphosphonate; alpha-halogenoalkylidenediphosphonate; chlorophosphate; halogen reagent; n-alkyllithium; ESTERS; ACID; PHOSPHONATES; TRANSFORMATIONS; DERIVATIVES; PHOSPHORUS; ANALOGS;

机译：α-硫代亚烷基二膦酸酯;α-卤代亚烷基二膦酸酯;氯磷酸盐;卤素试剂;正烷基锂;酯;酸;膦酸酯;转化;衍生物;磷;模拟;

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1. A facile approach for the synthesis of alpha-halogenated alkylidenediphosphonates by reaction of alkyllithium with chlorophosphate and halogen reagent [J] . Lai CB, Xi CJ, Feng YP Phosphorus, Sulfur, and Silicon and the Related Elements . 2004,第3期

机译：一种通过烷基锂与氯磷酸盐和卤素试剂反应合成α-卤代亚烷基二膦酸酯的简便方法
2. Uranium(IV) alkyl complexes of a rigid dianionic non-donor ligand: Synthesis and quantitative alkyl exchange reactions with alkyllithium reagents [J] . Andreychuk N.R., Ilango S., Vidjayacoumar B., Organometallics . 2013,第5期

机译：刚性双阴离子非供体配体的铀（IV）烷基络合物：烷基锂试剂的合成和定量烷基交换反应
3. Multi-step reactions of N-monosubstituted (polyfluoroalkane)thioamides with alkyllithium reagents [J] . Sergiy S.Mikhailichenko, Alexander V.Rudnichenko, Vadim M.Timoshenko Journal of Fluorine Chemistry . 2007,第7期

机译：N-单取代（聚氟烷烃）硫代酰胺与烷基锂试剂的多步反应
4. SYNTHESIS OF MoS2/Pd COMPOSITES VIA A FACILE SONOCHEMICAL APPROACH FOR OXYGEN REDUCTION REACTION [C] . Ling-Xia Zuo, Li-Ping Jiang, Jun-Jie Zhu ACS National Meeting Exhibition . 2016

机译：通过用于氧还原反应的容易的Sonochemical方法来合成MOS2 / Pd复合材料
5. REACTIONS OF ALKYLLITHIUM REAGENTS WITH HALOALKANES. [D] . GIBSON, GERALD WRAY. 1963

机译：烷基钾试剂与卤代烷的反应。
6. Polyol Synthesis with β-Oxyanionic Alkyllithium Reagents: Syntheses of Aculeatins A B and D [O] . Viengkham Malathong, Scott D. Rychnovsky -1

机译：多元醇合成β-含氧阴离子烷基锂试剂：aculeatins aB和d的合成
7. Reactions of 2,2,2-trichloroethylamines with Grignard reagents and alkyllithiums. [O] . MASANORI TAKAMATSU, YOSHIYASU TERAO, MINORU SEKIYA 1982

机译：2,2,2-三氯乙胺与格氏试剂和烷基锂的反应。
8. Reaction of Secondary and Tertiary Alkyllithium Reagents with Vinyl Di- and Trisiloxanes. Synthesis of alpha-Silyl Silanols [R] . Firgo, H. A., Weber, W. P. 1981

机译：二级和三级烷基锂试剂与乙烯基二硅氧烷和三硅氧烷的反应。 α-甲硅烷基硅烷醇的合成

A facile approach for the synthesis of alpha-halogenated alkylidenediphosphonates by reaction of alkyllithium with chlorophosphate and halogen reagent

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