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首页> 外文期刊>Phosphorus, Sulfur, and Silicon and the Related Elements >A facile and clean procedure for preparation of -aminophosphonates via a rotary evaporator equipped with circulating water vacuum pumps
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A facile and clean procedure for preparation of -aminophosphonates via a rotary evaporator equipped with circulating water vacuum pumps

机译:通过配备有循环水真空泵的旋转蒸发仪轻松而干净地制备-氨基膦酸酯

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摘要

RE-CWVP (rotary evaporator equipped with a circulating water vacuum pump)-assisted synthesis is reported as an extremely efficient, facile, and clean procedure for the preparation of -aminophosphonates in organic synthesis and industrial processes. The title -aminophosphonates are obtained in good to satisfactory yields by the method and characterized by means of IR, 1H NMR, 31P NMR, 13C NMR, and mass spectrometry.
机译:据报道,RE-CWVP(配备有循环水真空泵的旋转蒸发仪)辅助合成是一种在有机合成和工业过程中制备-氨基膦酸酯的极其有效,简便且清洁的方法。通过该方法以良好至令人满意的产率获得标题-氨基膦酸酯,并通过IR,1 H NMR,31 P NMR,13 C NMR和质谱进行表征。

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