Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates

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Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates

机译：色谱法和环保型芳基甲苯磺酸酯和甲磺酸酯的合成

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摘要

Two chromatography-free and eco-friendly protocols have been developed to synthesize aryl tosylates and mesylates by the tosylation and mesylation of the corresponding hydroxyarenes, respectively. These protocols are superior to other known ones regarding the simplicity, reaction time and conditions, the range of substrates, yields, and environmental friendliness.

机译：已经开发了两种无色谱法和环保的方案，分别通过相应羟基芳烃的甲苯磺酸化和甲磺酰化来合成芳基甲苯磺酸酯和甲磺酸酯。这些协议在简单性，反应时间和条件，底物范围，产率和环境友好性方面优于其他已知协议。

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《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2015年第17期|共8页
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正文语种 eng
中图分类化学;
关键词
aryl mesylates; aryl tosylates; green chemistry; mesylation; tosylation;

机译：甲苯磺酸芳基酯;甲苯磺酸芳基酯;绿色化学;甲基化;甲苯磺酸化;

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专利

1. Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates [J] . Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2015,第17期

机译：色谱法和环保型芳基甲苯磺酸酯和甲磺酸酯的合成
2. Synthesis of Unsymmetrical Diarylethynes by Pd(0)/Cu(I)-cocatalyzed Sila-Sonbgashira-Hagihara Coupling Reactions of Alkynylsilanes with Aryl Tosylates or Mesylates [J] . Yasushi Nishihara, Daisuke Ogawa, Shintaro Noyori Chemistry Letters . 2012,第11期

机译：Pd（0）/ Cu（I）催化的炔基硅烷与甲苯磺酸烷基酯或甲磺酸烷基酯的Sila-Sonbgashira-Hagihara偶联反应合成不对称二芳基乙炔
3. Palladium-Catalyzed Borylation of Aryl Mesylates and Tosylates and Their Applications in One-Pot Sequential Suzuki–Miyaura Biaryl Synthesis [J] . Wing Kin Chow Dr. Chau Ming So Prof. Dr. Chak Po Lau Prof. Dr. Fuk Yee Kwong Chemistry - A European Journal . 2011,第25期

机译：钯催化的甲磺酸烷基酯和甲苯磺酸酯的硼化反应及其在一锅顺序铃木-宫浦联芳的合成中的应用
4. Micro-reactor synthesis: synthesis of cyanobiphenyls using a modified suzuki coupling of an aryl halide and aryl boronic acid. [C] . Victoria Skelton, Gillian M.Greenway, Stephen J.Haswell, International conference on microreaction technology . 2000

机译：微反应器合成：使用芳基卤化物和芳族硼酸的改性铃木偶联来合成氰基苯基。
5. Aryl mesylates in nickel (0) catalyzed homo- and cross coupling reactions. [D] . Bae, Jin-Young. 1995

机译：镍（0）中的甲磺酸甲磺酸酯催化均相和交叉偶联反应。
6. STILLE CROSS-COUPLING REACTIONS OF ARYL MESYLATES AND TOSYLATES USING A BIARYLPHOSPHINE BASED CATALYST SYSTEM [O] . John R. Naber, Brett P. Fors, Xiaoxing Wu, -1

机译：sTILLE交叉偶联芳基甲磺酸酯并使用BIaRYLpHOspHINE基催化剂系统反应苯磺酸
7. Palladium-catalyzed borylation of aryl mesylates and tosylates and their applications in one-pot sequential Suzuki-Miyaura biaryl synthesis [O] . Chow WK, So CM, Lau CP, 2011

机译：钯催化的芳基甲磺酸酯和甲苯磺酸酯的硼化及其在一锅顺序铃木-宫浦联芳合成中的应用

Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates

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