A simple method for the preparation of glycosyl isothiocyanates

Kuhne M; Gyorgydeak Z; Lindhorst TK

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A simple method for the preparation of glycosyl isothiocyanates

机译：一种制备异硫氰酸糖基酯的简单方法

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摘要

Glycosyl isothiocyanates became accessible from the corresponding peracetylated sugars in one step, by application of trimethylsilyl isothiocyanate and a Lewis acid in dichloromethane at room temperature.

机译：通过在室温下在二氯甲烷中应用三甲基甲硅烷基异硫氰酸酯和路易斯酸，可从相应的过乙酰化糖中一步获得糖基异硫氰酸酯。

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《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2006年第6期|共3页
作者
Kuhne M; Gyorgydeak Z; Lindhorst TK;
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正文语种 eng
中图分类有机化学;
关键词
carbohydrates; isothiocyanates; disaccharides; anomeric purity; glycomimetics; DERIVATIVES; THIOUREA; GLYCALS;

机译：碳水化合物;异硫氰酸酯;二糖;异构体纯度;糖模拟物;衍生物;硫脲;乙二醇;

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1. A simple method for the preparation of glycosyl isothiocyanates [J] . Kuhne M, Gyorgydeak Z, Lindhorst TK Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2006,第6期

机译：一种制备异硫氰酸糖基酯的简单方法
2. One-pot preparation and activation of glycosyl trichloroacetimidates:operationally simple glycosylation induced by combined use of solid-supported,reactivity-opposing reagents [J] . Masato Oikawa, Tatsushi Tanaka, Naohiro Fukuda, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第21期

机译：一锅法制备和激活糖基三氯乙酰胺酸酯：通过结合使用固体支持的，具有反应活性的试剂诱导简单的糖基化操作
3. One-pot preparation and activation of glycosyl trichloroacetimidates:operationally simple glycosylation induced by combined use of solid-supported,reactivity-opposing reagents [J] . Masato Oikawa, Tatsushi Tanaka, Naohiro Fukuda, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第21期

机译：一锅法制备和激活糖基三氯乙酰胺酸酯：通过结合使用固体支持的，具有反应活性的试剂诱导简单的糖基化操作
4. STEREOELECTRONIC EFFECTS IN GLYCOSYL ISOTHIOCYANATES [C] . C. Sosa, R. Babiano, P. Cintas International Carbohydrate Symposium . 2018

机译：糖基异氰酸酯的立体电子效应
5. I. New Methodologies and Catalysts for the Diels—Alder Reaction II. Computational and Synthetic Studies Toward the Total Synthesis of (–)-Stenine III. Synthetic Studies Toward the Total Syntheses of N-Methyl Welwitindolinone C isothiocyanate and N-Methyl Welwitindolinone B isothiocyanate [D] . Cleary, Leah 2013

机译：I. Diels-Alder反应的新方法和催化剂II。对（-）-Stenine III完全合成的计算和综合研究。 N-甲基韦尔吲哚啉酮C异硫氰酸酯的总合成的合成研究
6. Rapid Batch Method for the Preparation of Fluorescein Isothiocyanate-Conjugated Antibody [O] . John V. Calcagno, Michael J. Sweeney, Helen C. Oels 1973

机译：快速分批法制备荧光素异硫氰酸酯偶联抗体
7. Reaction of amino acids with D-glycosyl- and D-gluconyl isothiocyanates. [O] . HIROSHI TAKAHASHI, KAZUYOSHI TAKEDA, NORIYUKI NIMURA, 1979

机译：氨基酸与D-糖基和D-葡聚糖异硫氰酸酯的反应。
8. Methods and Compositions for Treatment of Central Nervous System Injury with Isothiocyanates. [R] . Dash, P. K. 2005

机译：用异硫氰酸酯治疗中枢神经系统损伤的方法和组合物。

A simple method for the preparation of glycosyl isothiocyanates

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