Temperature Resolved X-ray Diffraction for the Investigation of the Phase Transitions of FOX-7

P.B.Kempa; M.Herrmann

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Temperature Resolved X-ray Diffraction for the Investigation of the Phase Transitions of FOX-7

机译：温度分辨X射线衍射研究FOX-7的相变

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The phase behavior of 1,1-Diamino-2,2-dinitroethylene (FOX-7) was investigated by means of temperature resolved X-ray powder diffraction.Three phases were observed,and alpha- and beta-FOX-7 were identified by X-ray diffraction.The following transition scheme was found:Heating: alpha ->beta -> gamma at 113 deg C (alpha->beta) and 173 deg C (beta->gamma) Cooling: alpha (+gamma) <- gamma between 50 and 75 deg C The alpha,beta-transition is completely reversible,and the gamma/alpha-transition on cooling revealed to be incomplete.A fourth phase which is described in literature was not found.

机译：通过温度分辨X射线粉末衍射研究了1,1-二氨基-2,2-二硝基乙烯（FOX-7）的相行为，观察到三相，并通过α-烯烃鉴定了α-和β-FOX-7 X射线衍射发现以下过渡方案：加热：α->β->γ在113摄氏度（alpha-> beta）和173摄氏度（beta->γ）冷却：α（+γ）<-在50到75摄氏度之间的γ是完全可逆的，冷却时的γ/α转变显示为不完全。文献中没有发现第四相。

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《Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems》 |2006年第6期|共5页
作者
P.B.Kempa; M.Herrmann;
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正文语种 eng
中图分类特种结构材料;
关键词
Phase transitions; FOX-7; Temperature resolved XRD;

机译：相变;FOX-7;温度分辨XRD;

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1. Temperature Resolved X-ray Diffraction for the Investigation of the Phase Transitions of FOX-7 [J] . P.B.Kempa, M.Herrmann Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems . 2006,第6期

机译：温度分辨X射线衍射研究FOX-7的相变
2. Temperature-jump time-resolved X-ray diffraction study of cubic-cubic phase-transition kinetics in thermotropic cubic mesogen 1,2-Bis(4'-n- alkoxybenzoyl)hydrazines (BABH-n) [J] . Mori H., Kutsumizu S., Saito K., Langmuir: The ACS Journal of Surfaces and Colloids . 2010,第14期

机译：热致立方型液晶元1,2-双（4'-n-烷氧基苯甲酰基）肼（BABH-n）中立方-立方相变动力学的跃迁时间分辨X射线衍射研究
3. Temperature-jump time-resolved X-ray diffraction study of cubic-cubic phase-transition kinetics in thermotropic cubic mesogen 1,2-Bis(4'-n- alkoxybenzoyl)hydrazines (BABH-n) [J] . Mori H., Kutsumizu S., Saito K., Langmuir: The ACS Journal of Surfaces and Colloids . 2010,第14期

机译：热致立方型液晶元1,2-双（4'-n-烷氧基苯甲酰基）肼（BABH-n）中立方-立方相变动力学的跃迁时间分辨X射线衍射研究
4. Phase transitions of FOX-7 investigated by temperature resolved X-ray diffraction [C] . P. B. Kempa, M. Herrmann European powder diffraction conference;EPDIC 12 . 2011

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6. Kinetics of the lamellar and hexagonal phase transitions in phosphatidylethanolamine. Time-resolved x-ray diffraction study using a microwave-induced temperature jump. [O] . M Caffrey, R L Magin, B Hummel, 1990

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Temperature Resolved X-ray Diffraction for the Investigation of the Phase Transitions of FOX-7

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