Microwave-promoted Michael addition in neat water: A rapid, efficient and green method for the preparation of acyclic nucleosides

Qu GR; Zhang ZG; Geng MW; Xia R; Zhao L; Guo HM

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Microwave-promoted Michael addition in neat water: A rapid, efficient and green method for the preparation of acyclic nucleosides

机译：微波促进纯净水中的迈克尔加成：一种快速，高效且绿色的无环核苷制备方法

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摘要

Syntheses of acyclic nucleosides were achieved in water with the aid of microwave irradiation, providing a rapid, efficient and convenient method for the preparation of acyclic nucleosides in high yields.

机译：无环核苷的合成是通过微波辐射在水中完成的，为快速，高效，方便地高产率制备无环核苷提供了方法。

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《Synlett》 |2007年第5期|共4页
作者
Qu GR; Zhang ZG; Geng MW; Xia R; Zhao L; Guo HM;
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正文语种 eng
中图分类有机化学;
关键词
acyclic nucleoside; microwave irradiation (MWI); Michael addition; green solvent; PURINE NUCLEOBASES; ORGANIC-SYNTHESIS; PYRIMIDINE; DERIVATIVES; INHIBITORS; ADENINE; ANALOGS; GUANINE; 9-(2-HYDROXYETHOXYMETHYL)GUANINE; IRRADIATION;

机译：无环核苷;微波辐照（MWI）;迈克尔加成;绿色溶剂;嘌呤核苷;有机合成;嘧啶;衍生物;抑制剂;腺嘌呤;类似物;鸟嘌呤;9-（2-羟基乙氧基甲基）鸟嘌呤;辐照;

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专利

1. Microwave-promoted Michael addition in neat water: A rapid, efficient and green method for the preparation of acyclic nucleosides [J] . Qu GR, Zhang ZG, Geng MW, Synlett . 2007,第5期

机译：微波促进纯净水中的迈克尔加成：一种快速，高效且绿色的无环核苷制备方法
2. KF/Al2O3 as a Highly Efficient, Green, Heterogeneous, and Reusable Catalytic System for the Solvent-Free Synthesis of Carboacyclic Nucleosides via Michael Addition Reaction [J] . Zare A, Hasaninejad A, Beyzavi MH, Synthetic Communications . 2009,第1a3期

机译：KF / Al2O3是高效，绿色，多相和可重复使用的催化体系，可通过迈克尔加成反应无溶剂合成碳环核苷
3. KF/Al2O3 as a Highly Efficient, Green, Heterogeneous, and Reusable Catalytic System for the Solvent-Free Synthesis of Carboacyclic Nucleosides via Michael Addition Reaction [J] . Zare A, Hasaninejad A, Beyzavi MH, Synthetic Communications . 2009,第1期

机译：KF / Al2O3是高效，绿色，多相和可重复使用的催化体系，可通过迈克尔加成反应无溶剂合成碳环核苷
4. The preparation of pH-and thermo-sensitive chitosan-based hydrogels by Michael-Type Addition Reaction [C] . Hong-Liang Wei, Cun-Cai Ma, Hui-Juan Chu, International conference on mechanical and electronics engineering . 2011

机译：通过迈克尔型加成反应制备pH和热敏壳聚糖基水凝胶
5. New synthetic methodologies for chemo-, stereo-, and regioselective 1,4-conjugate additions of organometallic reagents to Michael and extended Michael substrates and alkene halofunctionalization reactions. [D] . Dhakal, Ramesh Chandra. 2014

机译：将有机金属试剂化学，立体和区域选择性1,4-缀合物添加到Michael和扩展的Michael底物以及烯烃卤代官能化反应的新合成方法。
6. Michael Addition Reactions between Chiral Equivalents of a Nucleophilic Glycine and (S)- or (R)-3-(E)-Enoyl-4-phenyl-13-oxazolidin-2-ones as a General Method for Efficient Preparation of β-Substituted Pyroglutamic Acids. Case of Topographically Controlled Stereoselectivity [O] . Vadim A. Soloshonok*, Chaozhong Cai, Takeshi Yamada, -1

机译：亲核甘氨酸与（S）-或（R）-3-（E）-烯丙基 -4-苯基-13-恶唑烷-2-酮的手性当量之间的迈克尔加成反应作为有效制备的一般方法β-取代的焦谷氨酸地形控制立体选择性的情况
7. Ionic liquid-accelerated Michael addition of pyrimidine and purine nucleobases to α,β-unsaturated esters: a rapid approach to carboacyclic nucleosides synthesis [O] . Abdolkarim Zare, Alireza Hasaninejad, Roholla Safinejad, 2008

机译：离子液体加速迈克尔加入嘧啶和嘌呤核碱基到α，β-不饱和酯：碳环核苷合成的快速方法

Microwave-promoted Michael addition in neat water: A rapid, efficient and green method for the preparation of acyclic nucleosides

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