An Efficient and Convenient Procedure for Preparation of Diaryl Carbazone from aryl substituted carbazide

Yulu Wang; Lei Shi; Xueshun Jia; Feng Pan; Donglan Ma; Xiaoyang Wang

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An Efficient and Convenient Procedure for Preparation of Diaryl Carbazone from aryl substituted carbazide

机译：由芳基取代的咔嗪制备二芳基氨基甲酸酯的高效简便方法

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摘要

A new facile method for the synthesis of diaryl carbazone (ArN=NCONHNHAr) from aryl substituted carbazide is described. Eight of the compounds were preparated by oxidation of aryl substituted carbazide with ferric chloride in acid medium at room tempreture in good yield.

机译：描述了一种由芳基取代的咔嗪合成二芳基碳环（ArN = NCONHNHAr）的简便方法。在室温下，在酸性介质中，用氯化铁将芳基取代的咔嗪与氯化铁进行氧化，可制备出八种化合物，收率很高。

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《Synthetic Communications》 |1999年第1期|共4页
作者
Yulu Wang; Lei Shi; Xueshun Jia; Feng Pan; Donglan Ma; Xiaoyang Wang;
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正文语种 eng
中图分类有机化学;
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1. An Efficient and Convenient Procedure for Preparation of Diaryl Carbazone from aryl substituted carbazide [J] . Yulu Wang, Lei Shi, Xueshun Jia, Synthetic Communications . 1999,第1期

机译：由芳基取代的咔嗪制备二芳基氨基甲酸酯的高效简便方法
2. Selective and efficient oxidation of diaryl carbazide to diaryl carbazone with NaNO_2-acetic anhydride under mild conditions [J] . Xiao-Chuan Li, Yu-Lu Wang, Jin-Ye Wang Synthetic Communications . 2002,第21期

机译：NaNO_2-乙酸酐在温和条件下将二芳基咔嗪选择性和有效氧化为二芳基氨基甲酸
3. A convenient method for the preparation of carbonyl diazo compounds from aryl substituted carbazide [J] . Wang YL., Jia XS., Shi L. Synthetic Communications . 1998,第12期

机译：一种由芳基取代的咔嗪制备羰基重氮化合物的简便方法
4. Magnesium-Induced Copper-Catalyzed Preparation of Unsymmetrical Diaryl Sulfides from Aryl Iodides and Bisulfide Compounds via Cleavage of S-S Bond [C] . Nobukazu Taniguchi, Tetsuo Onami Symposium on Organometallic Chemistry . 2004

机译：镁催化铜催化的非对称二芳基硫化物制备来自芳基碘和双硫化物化合物的S-S键
5. Oxidative addition of aryl halides and sulfonates to palladium(0), and reductive elimination of aryl halides and diaryl ethers from palladium(II): Mechanistic investigations and synthetic applications. [D] . Roy, Amy Helen. 2003

机译：将芳基卤化物和磺酸盐氧化添加到钯（0）中，并从钯（II）中还原消除芳基卤化物和二芳基醚：机理研究和合成应用。
6. A convenient route to symmetrically and unsymmetrically substituted 35-diaryl-246-trimethylpyridines via Suzuki–Miyaura cross-coupling reaction [O] . Dariusz Błachut, Joanna Szawkało, Zbigniew Czarnocki 2016

机译：通过Suzuki-Miyaura交叉偶联反应制取对称和非对称取代的35-二芳基-246-三甲基吡啶的简便方法
7. CsOH/DMSO Promoted Reactions of Aryl Halides with Phenols: A Convenient Method for the Synthesis of Diaryl Ethers [O] . Pingliang Chen, Shijie Lu, Xingen Hu, 2014

机译：CSOH / DMSO促进芳基卤化物与酚的反应：一种合成二芳基醚的方法
8. Organophosphazenes. XIV. Para Substituted Aryl and Mixed Para Substituted Aryl/Phenyl Fluorocyclotriphosphazene Derivatives [R] . Allen, C. W., Brunst, G. E., Perlman, M. E. 1980

机译：有机磷腈。十四。对位取代的芳基和混合对位取代的芳基/苯基氟代环三磷腈衍生物

An Efficient and Convenient Procedure for Preparation of Diaryl Carbazone from aryl substituted carbazide

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