Solvent-free esterification of carboxylic acids and alcohols in the presence of silphos [PCl _(3-n)(SiO _2) _n] as a heterogeneous phosphine reagent

Rao A.N.; Ganesan K.; Shinde C.K.

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Solvent-free esterification of carboxylic acids and alcohols in the presence of silphos [PCl _(3-n)(SiO _2) _n] as a heterogeneous phosphine reagent

机译：在作为非均相膦试剂的silphos [PCl _（3-n）（SiO _2）_n]存在下，羧酸和醇的无溶剂酯化

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摘要

An efficient solvent-free method for the preparation of esters from various aromatic and aliphatic acids with primary, secondary, and tertiary alcohols using a heterogeneous phosphine reagent, silphos [PCl _(3-n)(SiO _2) _n], in good yields is reported.

机译：一种高效，无溶剂的方法，可以使用多相膦试剂silphos [PCl _（3-n）（SiO _2）_n]从各种芳族和脂肪酸与伯，仲和叔醇制备酯，产率高被报道。

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《Synthetic Communications》 |2012年第15期|共10页
作者
Rao A.N.; Ganesan K.; Shinde C.K.;
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正文语种 eng
中图分类有机化学;
关键词
Alcohols; carboxylic acids; esterification; heterogeneous; silphos;

机译：醇;羧酸;酯化;非均相;硅氧烷;

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专利

1. Solvent-Free Esterification of Carboxylic Acids and Alcohols in the Presence of Silphos [PCl_3-n(SiO₂)_n] as a Heterogeneous Phosphine Reagent [J] . Ambati Narasimha Rao, Chandra Kant Shinde Synthetic Communications: An International Journal for Rapid Communication of Synthetic Organic Chemistry . 2012,第15期

机译：Silphos [PCl _{3-n （SiO _{2 ）_{n ]作为非均相膦存在下的羧酸和醇的无溶剂酯化试剂}}}
2. Silphos [PCl_(3-n)(SiO_2)_n]:a heterogeneous phosphine reagent for formylation and acetylation of alcohols and amines with ethyl formate and acetate [J] . Nasser Iranpoor, Habib Firouzabadi, Arezu Jamalian Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2005,第46期

机译：Silphos [PCl_（3-n）（SiO_2）_n]：一种异质膦试剂，用于用甲酸乙酯和乙酸盐对醇和胺进行甲酰化和乙酰化
3. Silphos [PCl_(3-n)(SiO_2)_n]:a heterogeneous phosphine reagent for formylation and acetylation of alcohols and amines with ethyl formate and acetate [J] . Nasser Iranpoor, Habib Firouzabadi, Arezu Jamalian Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2005,第46期

机译：Silphos [PCl_（3-n）（SiO_2）_n]：一种异质膦试剂，用于用甲酸乙酯和乙酸盐对醇和胺进行甲酰化和乙酰化
4. Large-Scale Production of meta-Phenolsulfonic Acid-Formaldehyde Resin Catalyst for Continuous Flow Esterification ofVarious Carboxylic Acids and Alcohols [C] . Heeyoel Baek, Hao Hu, Hajime Ota 日本化学会春季年会 . 2020

机译：用于连续流动酯化的Meta-Phenolsulfonic酸甲酸甲醛树脂催化剂的大规模生产羧酸和醇
5. Uncatalyzed esterification of biomass-derived carboxylic acids [D] . Bankole, Kehinde Seun 2011

机译：生物质衍生羧酸的未催化酯化
6. Solvent-Free Esterification of Carboxylic Acids Using Supported Iron Oxide Nanoparticles as an Efficient and Recoverable Catalyst [O] . Fatemeh Rajabi, Mohammad Abdollahi, Rafael Luque 2016

机译：使用负载的氧化铁纳米粒子作为高效可回收的催化剂对羧酸进行无溶剂酯化
7. Solvent-Free Esterification of Carboxylic Acids Using Supported Iron Oxide Nanoparticles as an Efficient and Recoverable Catalyst [O] . Fatemeh Rajabi, Mohammad Abdollahi, Rafael Luque 2016

机译：使用负载型氧化铁纳米粒子作为有效和可回收的催化剂，无溶剂酯化羧酸

Solvent-free esterification of carboxylic acids and alcohols in the presence of silphos [PCl _(3-n)(SiO _2) _n] as a heterogeneous phosphine reagent

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