Efficient synthesis of novel 2,4-[diaryl-3-azabicyclo[3.3.1]nonan-9-yl]-5- spiro-4-acetyl-2-(acetylamino)-δ~2-1,3,4-thiadiazolines

Rani M.; Ramachandran R.; Kabilan S.

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Efficient synthesis of novel 2,4-[diaryl-3-azabicyclo[3.3.1]nonan-9-yl]-5- spiro-4-acetyl-2-(acetylamino)-δ~2-1,3,4-thiadiazolines

机译：新型2,4- [二芳基-3-氮杂双环[3.3.1]壬南-9-基] -5-螺-4-乙酰基-2-乙酰基-2-（乙酰氨基）-δ〜2-1,3,4-的高效合成噻二唑啉

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2,4-[Diaryl-3-azabicyclo[3.3.1]nonan-9-yl]-5-spiro-4-acetyl-2-(acetylamino) -2-1,3,4-thiadiazoline derivatives (3a-h) have been synthesized by the cyclization of 2,4-diaryl-3-azabicyclo[3.3.1]nonan-9-one thiosemicarbazones (2a-h) under acetylating condition. The synthesized compounds were characterized by analytical and spectral (infrared, 1H NMR, and 13C NMR) studies.

机译：2,4- [Diaryl-3-azabicyclo [3.3.1] nonan-9-yl] -5-spiro-4-acetyl-2-（acetylamino）-2-1,3,4-thiadiazoline衍生物（3a-h ）是通过在乙酰化条件下将2,4-二芳基-3-氮杂双环[3.3.1]壬南-9-硫代半氨基甲酮（2a-h）环化合成的。通过分析和光谱（红外，1 H NMR和13 C NMR）研究对合成的化合物进行表征。

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《Synthetic Communications》 |2010年第12期|共7页
作者
Rani M.; Ramachandran R.; Kabilan S.;
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正文语种 eng
中图分类有机化学;
关键词
Acetic anhydride; Azabicyclo3.3.1nonan-9-ones; Cyclization; Thiadiazolines; Thiosemicarbazones;

机译：乙酸酐;氮杂双环[3.3.1] nonan-9-ones;环化;噻二唑啉;硫代半氨基甲酮;

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1. Efficient synthesis of novel 2,4-[diaryl-3-azabicyclo[3.3.1]nonan-9-yl]-5- spiro-4-acetyl-2-(acetylamino)-δ~2-1,3,4-thiadiazolines [J] . Rani M., Ramachandran R., Kabilan S. Synthetic Communications . 2010,第10a12期

机译：新型2,4- [二芳基-3-氮杂双环[3.3.1]壬南-9-基] -5-螺-4-乙酰基-2-乙酰基-2-（乙酰氨基）-δ〜2-1,3,4-的高效合成噻二唑啉
2. Synthesis of 5-spiro(5'-methylisatin)-4-acetyl-2-(acetylamino)-#DELTA#~2-1,3,4-thiadiazoline and 5-spiro(5'-methylisatin)-4-acetyl-2-(5'-methylisatin-3'-hydrazino)-#DELTA#~2-1,3,4-thiadiazoine [J] . Rafiqul Islam, M Joynal Abedin, Khurshida Khayer, Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2001,第3期

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机译：螺[chromeno [4,3-d] [1,2,3]噻二唑-4,1'-环己烷，螺[chromeno [4,3-d] [1,2,3]硒二唑 - 的合成和抗菌活性4,1'-环己烷和螺[苯并二氢吡喃-2,1'-环己烷] -4-酮-5-螺-4-乙酰基-2-（乙酰氨基）-Δ2-1,3,4-噻二唑啉化合物

Efficient synthesis of novel 2,4-[diaryl-3-azabicyclo[3.3.1]nonan-9-yl]-5- spiro-4-acetyl-2-(acetylamino)-δ~2-1,3,4-thiadiazolines

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