One-step synthesis of tolunitriles by heterogeneously catalyzed liquid-phase ammoxidation

Liu Y; Zhong M; Yu W; Ma YL

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One-step synthesis of tolunitriles by heterogeneously catalyzed liquid-phase ammoxidation

机译：多相催化液相氨氧化一步合成甲苯二酚

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摘要

Tolunitriles have been efficiently synthesized by selective ammoxidation of corresponding xylene over silica-supported Co-Mn-Mg-Ni catalysts, without solvent for the first time in a one-pot procedure. The selectivity for mono-nitriles is almost 100%.

机译：通过在二氧化硅负载的Co-Mn-Mg-Ni催化剂上，在没有溶剂的情况下，将相应的二甲苯选择性氨氧化，可以有效地合成甲苯腈。单腈的选择性几乎为100％。

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来源
《Synthetic Communications》 |2005年第23期|共4页
作者
Liu Y; Zhong M; Yu W; Ma YL;
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正文语种 eng
中图分类有机化学;
关键词
ammoxidation; liquid-phase ammoxidation; tolunitrile; xylene; MILD CONDITIONS; NITRILES;

机译：氨氧化;液相氨氧化;甲苯磺酸;二甲苯;混合条件;腈;

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专利

1. One-step synthesis of tolunitriles by heterogeneously catalyzed liquid-phase ammoxidation [J] . Liu Y, Zhong M, Yu W, Synthetic Communications . 2005,第23期

机译：多相催化液相氨氧化一步合成甲苯二酚
2. Eco-friendly Synthesis of m-Tolunitrile by Heterogeneously Catalysed Liquid Phase Ammoxidation [J] . Min Zhong, Yong-guang Liang, Yuan Liu, Chemistry Letters . 2005,第5期

机译：非均相催化液相氨氧化技术环保合成间苯三酚
3. Synthesis of 4-Phenylphthalonitrile by Vapor-Phase Catalytic Ammoxidation of Intermediate 4-Phenyl-o-Tolunitrile: Reaction Kinetics [J] . G. A. Bagirzade, D. B. Tagiyev, M. R. Manafov Modern Research in Catalysis . 2014,第1期

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4. One-step Synthesis of Lemonile from Citral by Liquid Phase Catalytic Ammoxidation [C] . Ye Wang, Shaofeng Pi, Jinhua Zhou, International conference on biotechnology, chemical and materials engineering . 2013

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One-step synthesis of tolunitriles by heterogeneously catalyzed liquid-phase ammoxidation

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