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The effect of Ag wire shape on the microstructure and J(c) performance of BPSCCO-2223/Ag wire composite bulks

机译:银线形状对BPSCCO-2223 /银线复合材料的微观结构和J(c)性能的影响

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To improve the superconducting properties of (Bi,Pb)(2)Sr2Ca2Cu3Oy (BPSCCO-2223) superconductors, we investigate the microstructure and critical current density (J(c)) performance at 77.3 K under self-field and/or 4.2 K under several magnetic fields on BPSCCO-2223 bulk composed of silver (Ag) wires with diameters of 0.2 mm and 0.4 mm. The composites of Ag wires are hand-made by stacking Ag wires into the oxide powder in the direction of thickness alternately, and then the prepared samples are sintered at 840 degreesC for 50 h. In this study SEM and EPMA observation results show that good c-axis oriented and densely structured BPSCCO-2223 plate-like grains can be formed around the interfacial region between BPSCCO-2223 oxide and metal Ag regardless of the diameter of Ag wire. The J(c) values of the sample composed of Ag wires are higher than those of the sample without Ag wires. The J(c) values of the sample composed of 0.4 mm Ag wires are higher than those of the sample composed of 0.2 mm Ag wires, and then these values improved further by increasing the number of Ag wires regardless of their diameter under several measurement conditions. The maximum Jc values are estimated about 300 A cm(-2) at 77.3 K under self-field, and 1200 A cm-2 at 4.2 K under self-field when composed of 24 0.4 mm Ag wires. These J(c) values are about two to three times higher than those of the bulk without Ag wire. [References: 5]
机译:为了提高(Bi,Pb)(2)Sr2Ca2Cu3Oy(BPSCCO-2223)超导体的超导性能,我们研究了77.3 K,自电场和/或4.2 K下的微结构和临界电流密度(J(c))性能。 BPSCCO-2223主体上的几个磁场由直径为0.2毫米和0.4毫米的银(Ag)线组成。通过将Ag线沿厚度方向交替堆叠到氧化物粉末中来手工制作Ag线的复合材料,然后将制备的样品在840℃下烧结50 h。在这项研究中,SEM和EPMA的观察结果表明,无论Ag焊丝的直径如何,都能在BPSCCO-2223氧化物和金属Ag之间的界面区域周围形成良好的c轴取向和致密结构的BPSCCO-2223板状晶粒。由银线组成的样品的J(c)值高于无银线的样品的J(c)值。由0.4毫米银线组成的样品的J(c)值高于由0.2毫米银线组成的样品的J(c)值,然后通过增加银线的数量而不考虑其在几种测量条件下的直径,进一步提高了这些值。当由24条0.4 mm Ag线组成时,估计的最大Jc值在自电场下为77.3 K时约为300 A cm(-2),在自电场下为4.2 K时约为1200 A cm-2。这些J(c)值大约是没有银线的散装材料的J(c)值的两到三倍。 [参考:5]

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