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Preparation of mesoporous TiO_2/CNT nanocomposites by synthesis of mesoporous titania via EISA and their photocatalytic degradation under visible light irradiation

机译:EISA法合成介孔二氧化钛制备介孔TiO_2 / CNT纳米复合材料及其在可见光下的光催化降解

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摘要

Stabilized mesoporous TiO_2 was synthesized by evaporation induced self assembly (EISA) method and mechanically incorporated into single-walled carbon nanotubes (SWCNT) with different ratios. The physicochemical properties of the nanocomposites (mesoporous TiO_2/SWCNT) materials were investigated by Brunauer-Emmett-Teller (BET) measurement, X-ray diffraction (XRD), transmission electron microscopy (TEM), energy dispersive X-ray (EDX), photoluminescence (PL) and ultraviolet-visible (UV -Vis) spectroscopy measurements. The catalytic activity of mesoporous TiO_2 and nanocomposites were assessed by examining the degradation of rhodamine B as model aqueous solution under visible light. CNTs are facilitating the photocatalytic activity of mesoporous TiO_2 in the degradation of rhodamine B efficiently.
机译:通过蒸发诱导自组装(EISA)方法合成了稳定的介孔TiO_2,并以不同的比例将其机械结合到单壁碳纳米管(SWCNT)中。通过Brunauer-Emmett-Teller(BET)测量,X射线衍射(XRD),透射电子显微镜(TEM),能量色散X射线(EDX)来研究纳米复合材料(介孔TiO_2 / SWCNT)材料的理化性质。光致发光(PL)和紫外可见(UV -Vis)光谱测量。通过在可见光下检查作为模型水溶液的罗丹明B的降解来评估介孔TiO_2和纳米复合材料的催化活性。碳纳米管促进了中孔TiO_2的有效光催化罗丹明B降解。

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