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Polyaniline-polypyrrole coating for solid phase microextraction

机译:固相微萃取用聚苯胺-聚吡咯涂层

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摘要

A procedure for direct electrochemical deposition of polyaniline-polypyrrole blend coating on the surface of stainless steel wire was suggested.Incorporation of polyaniline and polypyrrole into the blend coating was confirmed by infrared spectroscopy.Key parameters(pyrrole,aniline,dopant and sulphuric acid concentrations and deposition potential)influencing the coating's mechanical stability and surface homogeneity were optimised and thermostability of the coating was investigated.A possibility to apply the coating as a new fibre for solid phase microextraction was demonstrated.The coating showed better selectivity toward aromatic,hydrophobic compounds.
机译:提出了在不锈钢丝表面直接电化学沉积聚苯胺-聚吡咯共混涂层的方法,通过红外光谱法确定了聚苯胺和聚吡咯掺入共混涂层中的关键参数(吡咯,苯胺,掺杂剂和硫酸的浓度和优化了影响涂层机械稳定性和表面均一性的沉积电位,并研究了涂层的热稳定性。证明了将涂层作为新型纤维用于固相微萃取的可能性,该涂层对芳族,疏水化合物具有更好的选择性。

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