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Microwave assisted extraction of essential oils from enzymatically pretreated lavender (Lavandula angustifolia Miller)~+

机译:微波辅助从酶处理过的薰衣草中提取精油的方法

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摘要

In this study, microwave assisted a hydrodistillation process (MWHD) of essential oils from lavender (Lavandula angustifolia Miller) was investigated. In order to examine any potential differences in essential oil extraction, the lavender flowers underwent enzymatic pretreatment. A 2~3 factorial design of experiments, combined with statistical methods of data analysis were used to optimize enzymatic pretreatment and to evaluate the influence of major variables (enzyme concentration, temperature and pH) on the performance of the microwave assisted extraction. Under optimal conditions, an extraction yield of 24 mg oil g~(-1) substrate was achieved (an increase by approximately 25% in comparison with the classic extraction conditions of conventional hydrodistillation). The main compounds of the essential oils obtained were analyzed and identified by gas chromatography coupled to mass spectrometry (GC-MS). Analyzing the data obtained indicated that the content of main compounds (linalool and linalyl acetate - 73%) was greater than that obtained by conventional extraction (67%).
机译:在这项研究中,研究了微波辅助熏衣草(Lavandula angustifolia Miller)精油的加氢蒸馏过程(MWHD)。为了检查精油提取中的任何潜在差异,对薰衣草花进行了酶预处理。使用2〜3个因子设计的实验,结合数据分析的统计方法,可以优化酶预处理,并评估主要变量(酶浓度,温度和pH)对微波辅助萃取性能的影响。在最佳条件下,获得了24 mg油g〜(-1)底物的提取率(与传统加氢蒸馏的经典提取条件相比,提高了约25%)。通过气相色谱-质谱联用(GC-MS)分析和鉴定了所得精油的主要化合物。分析获得的数据表明,主要化合物(芳樟醇和乙酸芳樟酯-73%)的含量高于常规提取方法(67%)。

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