首页> 外文期刊>Organic Preparations and Procedures International: The New Journal for Organic Synthesis >Preparation of 3-(2-Chloroethyl)-6,7,8,9-tetrahydro-9-hydroxy-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one, a Key Intermediate for the Synthesis of Paliperidone

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Preparation of 3-(2-Chloroethyl)-6,7,8,9-tetrahydro-9-hydroxy-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one, a Key Intermediate for the Synthesis of Paliperidone

机译：合成关键中间体3-（2-氯乙基）-6,7,8,9-四氢-9-羟基-2-甲基-4H-吡啶并[1,2-a]嘧啶-4-酮的制备帕潘立酮的

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《Organic Preparations and Procedures International: The New Journal for Organic Synthesis》 |2016年第3期|共7页
作者
Solanki Pavankumar V.; Uppelli Sekhar Babu; Sarode Ganesh G.; Kardile Pritesh B.; Bembalkarb Saroj R.; Mathad Vijayavitthal T.;
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正文语种 eng
中图分类有机化学;基本有机化学工业;
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1. Preparation of 3-(2-Chloroethyl)-6,7,8,9-tetrahydro-9-hydroxy-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one, a Key Intermediate for the Synthesis of Paliperidone [J] . Solanki Pavankumar V., Uppelli Sekhar Babu, Sarode Ganesh G., Organic Preparations and Procedures International: The New Journal for Organic Synthesis . 2016,第1a3期

机译：合成关键中间体3-（2-氯乙基）-6,7,8,9-四氢-9-羟基-2-甲基-4H-吡啶并[1,2-a]嘧啶-4-酮的制备帕潘立酮的
2. Improved Process for Preparation of (3R,4R)-3-(3,4-Dimethyl-4-piperidinyl)phenol, A Key Intermediate for the Synthesis of Alvimopan [J] . Beeravalli Ramalinga Reddy, Kikkuru Srirami Reddy, Manoj Kumar Dubey Organic process research & development . 2014,第1期

机译：制备（3R，4R）-3-（3,4-二甲基-4-哌啶基）苯酚的关键方法
3. Synthesis of enantiopure (R)-2-(4-methoxy-3-(3-methoxypropoxy)-benzyl)-3- methylbutanoic acid-a key intermediate for the preparation of Alisldren [J] . Natalia Andrushko, Vasyl Andrushko, Thomas Thyrann Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2008,第41期

机译：对映纯（R）-2-（4-甲氧基-3-（3-甲氧基丙氧基）-苄基）-3-甲基丁酸-制备Alisldren的关键中间体
4. Synthesis and Characterization of Ba_(0.5)Sr_(0.5)Co_(0.8)Fe_(0.2)O_(3-δ) for Intermediate Temperature Solid Oxide Fuel Cell Cathode by Solid-State Reaction, Pechini and Citrate-EDTA Complexing Methods [C] . I.-Ming Hung, Chen-Yu Laing International Symposium on Solid Oxide Fuel Cells . 2009

机译：通过固态反应，Pechini和柠檬酸盐 - EDTA络合方法对中间温度固体氧化物燃料电池阴极进行中间温度固体氧化物燃料电池阴极的Ba_（0.5）Sr_（0.5）Co_（0.2）O_（3-δ）的合成与表征
5. An application of the intramolecular Heck reaction: A new strategy in the synthesis of Hasubanan alkaloids. Preparation of unsymmetrical biaryls via the Stille cross-coupling reaction: Synthesis of highly functional intermediates towards the synthesis of vindoline. [D] . Frank, Anthony Joseph. 2002

机译：分子内Heck反应的应用：合成Hasubanan生物碱的新策略。通过Stille交叉偶联反应制备不对称的联芳基：合成高功能性中间体，合成长春新碱。
6. Nucleoside-3-phosphotriesters as key intermediates for the oligoribonucleotide synthesis. III. An improved preparation of nucleoside 3-phosphotriesters their 1H NMR characterization and new conditions for removal of 2-cyanoethyl group. [O] . R W Adamiak, M Z Barciszewska, E Biala, 1976

机译：核苷3-磷酸三酯作为寡核糖核苷酸合成的关键中间体。三改进的核苷3-磷酸三酯的制备它们的1H NMR表征和去除2-氰基乙基的新条件。
7. Paliperidone: 3-{2-[4-(6-fluoro-1,2-benzoxazol-3-yl)piperidin-1-yl]ethyl}-9-hydroxy-2-methyl-1,6,7,8,9,9a-hexahydropyrido[1,2-a]pyrimidin-4-one [O] . Betz, Richard, Gerber, Thomas, Hosten, Eric, 2011

机译：帕潘立酮：3- {2- [4-（6-氟-1,2-苯并恶唑-3-基）哌啶-1-基]乙基} -9-羟基-2-甲基-1,6,7,8， 9,9a-六氢吡啶并[1,2-a]嘧啶-4-一
8. The Toxicity of Single Doses of 1-(2-Chloroethyl)-3-(trans-4-Methylcyclohexyl)-1-Nitrosourea (NSC-95,441:MeCCNU) for the Rhesus Monkey (Macaca mulatta) and the Dog. [R] . 1971

机译：单剂量1-（2-氯乙基）-3-（反式-4-甲基环己基）-1-亚硝基脲（NsC-95,441：meCCNU）对恒河猴（macaca mulatta）和狗的毒性。

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