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Preparation of CdS/TiO2 nanotube arrays and the enhanced photocatalytic property

机译:CdS / TiO2纳米管阵列的制备及增强的光催化性能

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In this paper, a series of CdS/TiO2 NTs have been synthesized by SILAR method. The as-prepared CdS/TiO2 NTs have been analyzed by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectrometer (EDS), and ultraviolet-visible (UV-vis). And their photocatalytic activities have been investigated on the degradation of methylene blue under simulated solar light irradiation. XRD results indicate that TiO2 NTs were anatase phase, CdS nanoparticles were hexagonal phase. FESEM results indicate that low deposition concentration can keep the nanotubular structures. UV vis results indicate that CdS can be used to improve the absorbing capability of TiO2 NTs for visible light, and the content of CdS affects the band gap. Photocatalytic results indicate that CdS nanoparticles are conducive to improve the photocatalytic efficiency of TiO2 NTs, and the highest degradation rate can reach 93.8%. And the photocatalytic mechanism of CdS/TiO2 NTs to methylene blue is also described. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
机译:本文采用SILAR方法合成了一系列的CdS / TiO2 NTs。制备的CdS / TiO2 NTs已通过X射线衍射(XRD),场发射扫描电子显微镜(FESEM),能量色散光谱仪(EDS)和紫外可见光(UV-vis)进行了分析。研究了它们在模拟太阳光照射下对亚甲基蓝降解的光催化活性。 XRD结果表明TiO2 NTs为锐钛矿相,CdS纳米颗粒为六方相。 FESEM结果表明低沉积浓度可以保持纳米管结构。紫外可见结果表明,CdS可用于提高TiO2 NTs对可见光的吸收能力,并且CdS的含量会影响带隙。光催化结果表明,CdS纳米粒子有利于提高TiO2 NTs的光催化效率,最高降解率可达93.8%。并且还描述了CdS / TiO2 NTs对亚甲基蓝的光催化机理。 (C)2016 Elsevier Ltd和Techna Group S.r.l.版权所有。

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