Mn-mediated coupling of alkyl iodides and ketimines: A radical addition route to alpha,alpha-disubstituted alpha-aminoesters

Friestad GK; Ji A

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Mn-mediated coupling of alkyl iodides and ketimines: A radical addition route to alpha,alpha-disubstituted alpha-aminoesters

机译：Mn介导的烷基碘与酮亚胺的偶联：向α，α-二取代的α-氨基酯的自由基加成途径

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摘要

Coupling of primary and secondary alkyl iodides with N-acylhydrazonoesters via Mn-mediated photolysis conditions affords access to tert-alkyl amines.

机译：经由Mn介导的光解条件将伯烷基碘和仲烷基碘与N-酰肼基酯偶联，可获得叔烷基胺。

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《Organic letters》 |2008年第11期|共3页
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Friestad GK; Ji A;
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正文语种 eng
中图分类有机化学;
关键词
CHIRAL N-ACYLHYDRAZONES; ASYMMETRIC AMINE SYNTHESIS; CARBON-CENTERED RADICALS; ENANTIOSELECTIVE ALLYLATION; INTERMOLECULAR ADDITION; ACID-DERIVATIVES; C=N BOND; IMINES; CROTYLATION; HYDRAZONES;

机译：手性N-酰基氢;不对称胺的合成;碳中心自由基;对映选择性烯化;分子间加成;酸衍生物;C = N键;亚胺;CROCYLATION;HYDRAZONE;

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专利

1. Mn-mediated coupling of alkyl iodides and ketimines: A radical addition route to alpha,alpha-disubstituted alpha-aminoesters [J] . Friestad GK, Ji A Organic letters . 2008,第11期

机译：Mn介导的烷基碘与酮亚胺的偶联：向α，α-二取代的α-氨基酯的自由基加成途径
2. Mn-mediated coupling of alkyl iodides and chiral N-acylhydrazones: Optimization, scope, and evidence for a radical mechanism [J] . Friestad GK, Marie JC, Suh YS, The Journal of Organic Chemistry . 2006,第18期

机译：Mn介导的烷基碘与手性N-酰基hydr的偶联：优化，范围和自由基机理的证据
3. AIBN-initiated radical addition of gem-difluorinated alkyl iodides to alkynes and the Pd-catalyzed Sonogashira coupling reaction of E-phenyl difluoromethylene vinylic iodides with terminal alkynes [J] . Xiang Fang, Xueyan Yang, Xianjin Yang, Tetrahedron . 2007,第43期

机译：AIBN引发的将二氟代烷基碘加到炔烃中，以及Pd催化的E-苯基二氟亚甲基乙烯基碘化物与末端炔烃的Sonogashira偶联反应
4. Alkyl Radical Stability from the Decomposition and Isomerization of Primary Iodides: 5-Methyl-Hexyl Radical from 5-Methyl-Hexyl Iodide [C] . Iftikhar A. Awan, Wing Tsang, W. Sean McGivern, US Combustion Meeting; 20070325-28; San Diego,CA(US) . 2007

机译：伯碘化物分解和异构化产生的烷基自由基稳定性：来自5-甲基己基碘化物的5-甲基己基自由基
5. Mn-mediated radical coupling toward synthesis of alpha,alpha-disubstituted alpha-amino esters and formal synthesis of quinine. [D] . Ji, An. 2011

机译：Mn介导的自由基偶联，可合成α，α-二取代的α-氨基酯和奎宁。
6. Stereoselective Access to Tubuphenylalanine and Tubuvaline: Improved Mn-Mediated Radical Additions and Assembly of A Tubulysin Tetrapeptide Analog [O] . Gregory K. Friestad, Koushik Banerjee, Jean-Charles Marié, -1

机译：立体选择性访问Tubuphenylalanine和Tubuvaline：改进的Mn介导的自由基加成和Tubulysin四肽类似物的组装。
7. Mn-Mediated Coupling of Alkyl Iodides and Chiral N-Acylhydrazones: Optimization, Scope, and Evidence for a Radical Mechanism [O] . -1

机译：Mn介导的烷基碘和手性N-酰腙的偶联：优化，范围和自由基机制的证据

Mn-mediated coupling of alkyl iodides and ketimines: A radical addition route to alpha,alpha-disubstituted alpha-aminoesters

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