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Preparation of SiO2 aerogel from rice husk ash

机译:用稻壳灰制备SiO2气凝胶

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Silica was leached from rice husk ash as sodium silicate by NaOH treatment. Using water glass as the silica source, SiO2 aerogel was prepared via the sol-gel process and supercritical drying of ethanol. Based on gelation time and porous characteristics of SiO2 aerogel, the optimum gel preparation technology was determined such as silica concentration of 6.0 wt%, gelation at pH value of 5.0 and aging in H2O/EtOH. Incidentally, the density was as low as 0.0713 g cm(-3), specific surface area was 729.82 m(2) g(-1), hole size was 3.39 cm(3) g(-1), and average pore size was 16.32 nm, and the size distribution was uniform.
机译:通过NaOH处理从稻壳灰中以硅酸钠的形式浸出二氧化硅。使用水玻璃作为二氧化硅源,通过溶胶-凝胶工艺和乙醇超临界干燥制备了SiO2气凝胶。根据凝胶化时间和SiO2气凝胶的多孔特性,确定了最佳的凝胶制备技术,例如二氧化硅浓度为6.0 wt%,pH值为5.0时发生凝胶化以及在H2O / EtOH中老化。顺便说一下,密度低至0.0713 g cm(-3),比表面积为729.82 m(2)g(-1),孔尺寸为3.39 cm(3)g(-1),平均孔径为16.32nm,并且尺寸分布是均匀的。

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