Stable ruthenium nitrosyl porphyrins with axial O-bonded ligands; Preparation and redox behavior

Awasabisah D.; Xu N.; Sharmah Gautam K.P.Powell D.R.Shaw M.J.Richter-Addo G.B.

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Stable ruthenium nitrosyl porphyrins with axial O-bonded ligands; Preparation and redox behavior

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摘要

The six-coordinate compounds, (T(p-OMe)PP)Ru(NO)(OC_6HF _4) and (T(p-OMe)PP)Ru(NO)(OC(O)CF_3) have been prepared and characterized by IR and NMR spectroscopy, electrochemistry and IR spectroelectrochemistry, and by X-ray crystallography. These compounds undergo macrocycle-centered oxidations, and loss of axial ligands upon reduction.

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《Dalton transactions: An international journal of inorganic chemistry 》 |2013年第24期| 8537-8540| 共4页
作者
Awasabisah D.; Xu N.; Sharmah Gautam K.P.Powell D.R.Shaw M.J.Richter-Addo G.B.;
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作者单位

Department of Chemistry and Biochemistry, University of Oklahoma, Stephenson Life Sciences Research Center, 101 Stephenson Parkway, Norman OK 73019, United States;

Department of Chemistry, Southern Illinois University Edwardsville, Box 1652, Edwardsville IL 62026, United States;

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正文语种英语
中图分类化学 ;
关键词
ruthenium; porphyrins; redox;

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机译：Redox properties of ruthenium nitrosyl porphyrin complexes with different axial ligation: Structural, spectroelectrochemical (IR, UV-Visible, and EPR), and theoretical studies
2. SYNTHESIS, CHARACTERIZATION, AND ELECTROCHEMISTRY OF RUTHENIUM PORPHYRINS CONTAINING A NITROSYL AXIAL LIGAND [J] . Kadish KM., Vancaemelbecke E., Tan Z.Tagliatesta P.Bianco P.Boschi T.Yi GB.Khan MA.Richteraddo GB.Adamian VA. Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 1996 ,第5期

机译：SYNTHESIS, CHARACTERIZATION, AND ELECTROCHEMISTRY OF RUTHENIUM PORPHYRINS CONTAINING A NITROSYL AXIAL LIGAND
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机译：Photolabile Ruthenium Nitrosyls with Planar Dicarboxamide Tetradentate N_4 Ligands:Effects of In-Plane and Axial Ligand Strength on NO Release
4. Asymmetric cyclopropanation of styrene with ethyl diazoacetate using a N2P2-ligand ruthenium(II) catalyst:axial ligand controlled enantioselectivity [O] . 郑卓, 姚晓泉, 李琛, 2001

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Stable ruthenium nitrosyl porphyrins with axial O-bonded ligands; Preparation and redox behavior

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