Efficient reaction control through temperature and pressure measurement during microwave digestion

Dieter Gutwerk; Rainer Kramer

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Efficient reaction control through temperature and pressure measurement during microwave digestion

机译：通过微波消解过程中的温度和压力测量进行有效的反应控制

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Microwave digestion is one of the standard sample preparation procedures for elemental determination in analytical chemistry.In closed microwave-transparent pressure vessels the samples are heated together with a suitable acid solution to temperatures that are typically between 200 deg C and 260 deg C so that the sample is completely degraded and dissolved.

机译：微波消解是用于分析化学中元素测定的标准样品制备程序之一。在密闭的微波透明压力容器中，将样品与合适的酸溶液一起加热至通常在200摄氏度至260摄氏度之间的温度，以便样品完全降解并溶解。

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《Lab plus international》 |2006年第4期|共4页
作者
Dieter Gutwerk; Rainer Kramer;
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1. Efficient reaction control through temperature and pressure measurement during microwave digestion [J] . Dieter Gutwerk, Rainer Kramer Lab plus international . 2006,第4期

机译：通过微波消解过程中的温度和压力测量进行有效的反应控制
2. New technology for in situ visualization, monitoring and controlling microwave chemical reaction progress using a focused microwave high pressure–temperature closed-vessel digestion system [J] . Henryk Matusiewicz The Analyst . 2009,第7期

机译：利用聚焦微波高压-高温密闭容器消化系统原位可视化，监测和控制微波化学反应进程的新技术
3. New technology for in situ visualization, monitoring and controlling microwave chemical reaction progress using a focused microwave high pressure-temperature closed-vessel digestion system [J] . Henryk Matusiewicz The Analyst: The Analytical Journal of the Royal Society of Chemistry: A Monthly International Publication Dealing with All Branches of Analytical Chemistry . 2009,第7期

机译：利用聚焦微波高压高温密闭容器消化系统原位可视化，监测和控制微波化学反应进程的新技术
4. Efficient and High-Throughput Protein Digestion in Microwave-Assisted Enzymatic Reaction with Water Bubbling System [C] . Hyunjung Seo, Dong Min Kim, Yongha In, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2012

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5. Reactions of iron oxides at elevated pressures and temperatures. [D] . Labuda, Ewa. 1996

机译：氧化铁在高压和高温下的反应。
6. Structural-Controlled Synthesis of Highly Efficient Visible Light TiO2 Photocatalyst via One-Step Single-Mode Microwave Assisted Reaction [O] . Kunihiko Kato, Yunzi Xin, Takashi Shirai -1

机译：一步式单模微波辅助反应的结构控制合成高效可见光TiO2光催化剂
7. In situ temperature measurements in microwave-heated gas-solid catalytic systems. Detection of hot spots and solid-fluid temperature gradients in the ethylene epoxidation reaction [O] . Adrian Ramirez, Jose L. Hueso, Reyes Mallada, 2017

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Efficient reaction control through temperature and pressure measurement during microwave digestion

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